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Chemical Structure| 822-48-0 Chemical Structure| 822-48-0

Structure of 822-48-0

Chemical Structure| 822-48-0

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Product Details of [ 822-48-0 ]

CAS No. :822-48-0
Formula : C5H9ClO
M.W : 120.58
SMILES Code : CC1(CCl)COC1
MDL No. :MFCD01709552
InChI Key :MCZYEFODKAZWIH-UHFFFAOYSA-N
Pubchem ID :79112

Safety of [ 822-48-0 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H225-H302
Precautionary Statements:P210-P233-P240-P241+P242+P243-P264-P270-P280-P301+P312+P330-P303+P361+P353-P403+P235-P501
Class:3
UN#:1993
Packing Group:

Application In Synthesis of [ 822-48-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 822-48-0 ]

[ 822-48-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 822-48-0 ]
  • [ 4981-66-2 ]
  • 9,10-bis((3-methyloxetan-3-yl)methyloxy)anthracene [ No CAS ]
YieldReaction ConditionsOperation in experiment
45% With sodium hydroxide; In N,N-dimethyl acetamide; water; at 60℃; for 5h;Inert atmosphere; Synthesis of 9,10-bis {(3-methyloxetan-3-yl) methyloxy} anthracene A thermometer,In a three-necked flask equipped with a stirrer, 2.39 g (11.4 mmol) of 9,10-dihydroxyanthracene,3.6 g (30 mmol) of 3-chloromethyl-3-methyloxetane and 15 g of N, N-dimethylacetamide were added under a nitrogen atmosphere,To the resulting yellow-green solution was added 1.2 g of caustic soda and 6 g of water in water. It quickly turned into a reddish solution.Then,After heating at 60 ° C. for 5 hours,It became a skin color slurry.After cooling to room temperature,Suction filtrationWashingMethanol washing.The obtained wet cake was dried,1.94 g (5.1 mmol) of pale white crystals of 9,10-bis {(3-methyloxetan-3-yl) methyloxy} anthracene was obtained.The isolated yield based on the raw material 9,10-dihydroxyanthracene was 45 molpercent.
 

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