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Chemical Structure| 824-91-9 Chemical Structure| 824-91-9

Structure of 824-91-9

Chemical Structure| 824-91-9

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Product Details of [ 824-91-9 ]

CAS No. :824-91-9
Formula : C8H10O2
M.W : 138.16
SMILES Code : COCOC1=CC=CC=C1
MDL No. :MFCD00457267

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Application In Synthesis of [ 824-91-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 824-91-9 ]

[ 824-91-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 121-43-7 ]
  • [ 824-91-9 ]
  • [ 115377-93-0 ]
  • C16H19BO5 [ No CAS ]
  • 2
  • [ 824-91-9 ]
  • [ 115377-93-0 ]
YieldReaction ConditionsOperation in experiment
26 g N-BuLi (2.5 M, 96 ml) was added to a THF (250 ml) solution of Compound 3 (30 g, 220 mmol) at 0 C.Stir at 30 C. for 1 hour.To this solution was added B (OiPr) 3 (123 g, 651 mmol) at -78 C.The mixture was stirred at 30 C. for 2 hours to obtain a white suspension.Hydrochloric acid (1M) was added to adjust to pH = 6-7, and the organic layer was concentrated to obtain a mixture.The resulting mixture was washed with petroleum ether (80 ml) to obtain 26 g of compound 5.
 

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