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Chemical Structure| 838892-96-9 Chemical Structure| 838892-96-9

Structure of 838892-96-9

Chemical Structure| 838892-96-9

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Product Details of [ 838892-96-9 ]

CAS No. :838892-96-9
Formula : C13H10N2O2S
M.W : 258.30
SMILES Code : O=C1N(CC2=CN=C(C)S2)C(C3=C1C=CC=C3)=O

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Application In Synthesis of [ 838892-96-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 838892-96-9 ]

[ 838892-96-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 838892-96-9 ]
  • [ 63139-97-9 ]
YieldReaction ConditionsOperation in experiment
61% Suspend 2- (2-METHYLTHIAZOL-5-YLMETHYL) ISOINDOLE-1, 3-dione (210 MG, D. 814 mmol) in 6N HCl (8 mL) and heat at reflux for 2.5 hours. Cool to room temperature and stir for an additional 5 hours. Basify the mixture with 2 N sodium hydroxide, extract with methylene chloride (3 x 50 mL), dry (sodium sulfate), filter, and concentrate to afford 70 mg (61% yield) of the title compound as a brown OIL. H NMR (CDC13) 6 7.34 (s, 1H), 4.11 (s, 2H), 2.45 (S, 3H), 1.70 (br s, 2H).
 

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