Home Cart Sign in  
Chemical Structure| 87330-27-6 Chemical Structure| 87330-27-6

Structure of 87330-27-6

Chemical Structure| 87330-27-6

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 87330-27-6 ]

CAS No. :87330-27-6
Formula : C12H8N2O2
M.W : 212.20
SMILES Code : O=C1C=CNC2C1=CC=C1C=2NC=CC1=O
MDL No. :MFCD01548697
Boiling Point : No data available
InChI Key :SLIBCJURSADKPV-UHFFFAOYSA-N
Pubchem ID :77524

Safety of [ 87330-27-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Application In Synthesis of [ 87330-27-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 87330-27-6 ]
  • Downstream synthetic route of [ 87330-27-6 ]

[ 87330-27-6 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 87330-27-6 ]
  • [ 156492-30-7 ]
YieldReaction ConditionsOperation in experiment
70% With phosphorus(V) oxybromide In chloroform for 6 h; Inert atmosphere; Reflux 73c (4.2 g, 20 mmol),Tribromophosphine (14.3 g, 50 mmol),Dissolved in dry chloroform,Under nitrogen protection,Reflux for 6 hours,The reaction solution was washed with water,Saturated brine were washed three times,Dried over anhydrous magnesium sulfate,The solvent was evaporated,Purification by silica gel column chromatography gave compound 73d (4.7 g, 13.9 mmol)Yield 70percent
References: [1] Patent: CN106831743, 2017, A, . Location in patent: Paragraph 0129; 0134; 0135.
[2] Journal of Organic Chemistry, 1951, vol. 16, p. 941,945.
[3] Tetrahedron, 2002, vol. 58, # 44, p. 9095 - 9100.
 

Historical Records

Technical Information

Categories