Home Cart Sign in  
Chemical Structure| 874013-98-6 Chemical Structure| 874013-98-6

Structure of 874013-98-6

Chemical Structure| 874013-98-6

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 874013-98-6 ]

CAS No. :874013-98-6
Formula : C9H9ClN2
M.W : 180.63
SMILES Code : CC1=C(C)NC2=C1C=CN=C2Cl
MDL No. :MFCD22045096

Safety of [ 874013-98-6 ]

Application In Synthesis of [ 874013-98-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 874013-98-6 ]

[ 874013-98-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 874013-98-6 ]
  • [ 771574-00-6 ]
  • N-(4-fluoro-2-methylbenzyl)-2,3-dimethyl-1H-pyrrolo[2,3-c]pyridine-7-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
48% at 180.0℃; for 0.5h;Microwave irradiation; General procedure: A mixture of 4 (200 mg, 1.1 mmol) and benzylamine (1 mL,9.2 mmol) was stirred at 180 C for 30 min under microwave irradiation. The mixture was cooled to room temperature (rt). A saturated aqueous sodium hydrogen carbonate solution was added to the reaction mixture which was then extracted with EtOAc. The extract was washed successively with a saturated aqueous sodium hydrogen carbonate solution, and brine, dried over anhydrous sodium sulfate, and concentrated under reduced pressure. The residue was purified by silica gel column chromatography (eluent: hexane-EtOAc= 2 : 1) and the obtained solid was crystallized from IPE to give the title compound as a colorless solid (154 mg, 0.61 mmol, 56%).
 

Historical Records

Technical Information

Categories