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Chemical Structure| 877-24-7 Chemical Structure| 877-24-7
Chemical Structure| 877-24-7

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Product Details of Potassium Hydrogen Phthalate

CAS No. :877-24-7
Formula : C8H5KO4
M.W : 204.22
SMILES Code : O=C(O)C1=CC=CC=C1C([O-])=O.[K+]
MDL No. :MFCD00013070
InChI Key :IWZKICVEHNUQTL-UHFFFAOYSA-M
Pubchem ID :23676735

Safety of Potassium Hydrogen Phthalate

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of Potassium Hydrogen Phthalate

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 877-24-7 ]

[ 877-24-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 116754-58-6 ]
  • [ 877-24-7 ]
  • 2-(13-hydroxytridecyl)-1H-isoindole-1,3(2H)-dione [ No CAS ]
YieldReaction ConditionsOperation in experiment
With N,N-dimethyl-formamide; at 70℃; for 12h;Inert atmosphere; <strong>[116754-58-6]13-bromotridecan-1-ol</strong> 11(4.854 g, 17.4 mmcl) and potassium phthalate (4.311 g, 23.0 mmcl) were dissolved in anhydrous DMF (50 mL) under nitrogen gas. The reaction was stirred at 70C for 12 hours. The mixture was diluted with water and extracted into ethylacetate (3 x 200 mL). The combined extracts were washed with brine and dried oversodium sulfate. The solvent was removed in vacuo to yield 6.059g of a crude product.1H NMR (500 MHz, CDCI3): O 7.85-7.83 (m, 2H), 7.72-7.70 (m, 2H), 3.75-7.60 (m, 4H),1.67 (p, J= 7.0 Hz, 2H), 1.57 (p, J= 6.5 Hz, 2H), 1.40-1.20 (m, 18H).
 

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