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Chemical Structure| 877-89-4 Chemical Structure| 877-89-4

Structure of 877-89-4

Chemical Structure| 877-89-4

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Product Details of [ 877-89-4 ]

CAS No. :877-89-4
Formula : C6H9N3O3
M.W : 171.15
SMILES Code : COC1=NC(OC)=NC(OC)=N1
MDL No. :MFCD00142809
InChI Key :DFUGJTBMQKRCPI-UHFFFAOYSA-N
Pubchem ID :13419

Safety of [ 877-89-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 877-89-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 877-89-4 ]
  • Downstream synthetic route of [ 877-89-4 ]

[ 877-89-4 ] Synthesis Path-Upstream   1~2

  • 1
  • [ 877-89-4 ]
  • [ 16370-63-1 ]
YieldReaction ConditionsOperation in experiment
86% With ammonia In water at 25 - 51℃; for 2 h; Example 3A
Preparation of 2-amino-4,6-dimethoxy-1,3,5-triazine precursor
A mixture of 10.1 g (0.059 mole) of 2,4,6-trimethoxy-1,3,5-triazine and water (100 mL) was stirred at 25° C. while 110 mL of 28percent aqueous ammonia was added.
The mixture was held at 48-51° C. for two hours before it was cooled to 25° C. and the insoluble white crystals were removed.
The product was washed with water and dried to give 7.84 g (86percent), mp 218-221° C. 1H NMR (DMSO-d): 3.81 (s, 6H); 7.38 (s, 2H).
13C NMR (DMSO-d6): 53.9, 169.0, 171.9.
References: [1] Patent: US6833454, 2004, B1, . Location in patent: Page column 6-7.
[2] Chemische Berichte, 1886, vol. 19, p. 2072.
[3] Chemische Berichte, 1870, vol. 3, p. 271.
  • 2
  • [ 124-41-4 ]
  • [ 506-77-4 ]
  • [ 16370-63-1 ]
  • [ 877-89-4 ]
References: [1] Chemische Berichte, 1870, vol. 3, p. 271.
 

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[ 877-89-4 ]

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Related Parent Nucleus of
[ 877-89-4 ]

Triazines

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