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Chemical Structure| 897921-63-0 Chemical Structure| 897921-63-0

Structure of 897921-63-0

Chemical Structure| 897921-63-0

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Product Details of [ 897921-63-0 ]

CAS No. :897921-63-0
Formula : C30H23N
M.W : 397.51
SMILES Code : C1(C2=CC=C(C3=CC=CC=C3)C=C2)=CC=C(NC4=CC=C(C5=CC=CC=C5)C=C4)C=C1
MDL No. :MFCD34574539
InChI Key :MAOFYQZGOHNLTP-UHFFFAOYSA-N
Pubchem ID :58050462

Safety of [ 897921-63-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 897921-63-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 897921-63-0 ]

[ 897921-63-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 50548-45-3 ]
  • [ 897921-63-0 ]
  • C42H29NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
82% With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate; In 5,5-dimethyl-1,3-cyclohexadiene; for 6h;Inert atmosphere; Reflux; To a 500 ml round bottom flask in a nitrogen atmosphereCompound 1-Bromobenzofuran (10.0 g, 40.65 mmol),N - ([1,1'-biphenyl] -4-yl) - [1,1 ': 4', 1 '' - terphenyl]-4-amine ((N - ([1,1'-biphenyl] -4-yl) - [1,1 ': 4', 1 '' - terphenyl]-4-amine)(17.75 g, 44.72 mmol)Xylene(Xylene)After completely dissolved Sodium tert-butoxide(sodium tert-butoxide)(5.08 g, 52.85 mol) was added,Bis (tri-tert-butylphosphine) palladium (0)(Bis (tri-tert-butylphosphine) palladium (0)) (0.21 g, 0.41 mmol)And the mixture was heated and stirred for 6 hours. After the temperature was lowered to room temperature and the salts were removed by filtration, the xylene was concentrated under reduced pressure and recrystallized from ethyl acetate (250 ml) to obtain Compound (4) (18.89 g, yield: 82%)
 

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