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Chemical Structure| 90-76-6 Chemical Structure| 90-76-6

Structure of 90-76-6

Chemical Structure| 90-76-6

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Product Details of [ 90-76-6 ]

CAS No. :90-76-6
Formula : C6H13NO5
M.W : 179.17
SMILES Code : OC1[C@H](N)[C@H]([C@H]([C@@H](CO)O1)O)O
MDL No. :MFCD09954520

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Application In Synthesis of [ 90-76-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 90-76-6 ]

[ 90-76-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 90-76-6 ]
  • [ 63521-92-6 ]
  • [ 172946-61-1 ]
YieldReaction ConditionsOperation in experiment
49% To a solution of sodium methoxide (82 mL, 41 .0 mmol) in methanol was added 2-amino-2- deoxy-a-D-glucopyranose (7 g, 39.1 mmol). The mixture was stirred at room temperature for 45 min. The precipitated NaCI was removed by filtration through celite and the filter cake was rinsed with methanol (10 mL). The filtrate was placed in an ice-bath and pent-4-enoic anhydride (8.57 mL, 46.9 mmol) was added. The mixture was stirred for 30 min then kept at -10 C overnight. The precipitate was filtered, rinsed with methanol, and dried in vacuo to provide the amide 6a (5.01 g, 49%).
 

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