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Chemical Structure| 90929-73-0 Chemical Structure| 90929-73-0

Structure of 90929-73-0

Chemical Structure| 90929-73-0

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Product Details of [ 90929-73-0 ]

CAS No. :90929-73-0
Formula : C9H7BrN2O
M.W : 239.07
SMILES Code : BrCC(=O)C1=CNC2=NC=CC=C12
MDL No. :MFCD09265687

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Application In Synthesis of [ 90929-73-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 90929-73-0 ]

[ 90929-73-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 90929-73-0 ]
  • [ 89226-13-1 ]
  • [ 1001412-80-1 ]
YieldReaction ConditionsOperation in experiment
81% In acetonitrile; at 20 - 80℃; for 22h; Compound 14.1 (0.308 grams, 1.28 mmol) was mixed with Compound 14.2 (0.245 grams, 1.28 ramol) and AcCN (6 ml) was added. The reaction was stirred at ambient temperature for 20 hours followed by 80 C for 2 hours. The mixture was cooled to room temperature, diluted with EtOAc, washed with saturated sodium bicarbonate, brine, dried over sodium sulfate, filtered, and concentrated to yield Compound 14.3 (0.344 grams, 1.04 mmol, 81 %). ES (+) MS m/e = 331 (M+l).
  • 2
  • [ 2362-63-2 ]
  • [ 90929-73-0 ]
  • [ 1314082-86-4 ]
 

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