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Chemical Structure| 91298-74-7 Chemical Structure| 91298-74-7

Structure of 91298-74-7

Chemical Structure| 91298-74-7

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Product Details of [ 91298-74-7 ]

CAS No. :91298-74-7
Formula : C9H13NO
M.W : 151.21
SMILES Code : COC[C@@H](N)C1=CC=CC=C1
MDL No. :MFCD01862273
InChI Key :CMTDMIYJXVBUDX-SECBINFHSA-N
Pubchem ID :11768756

Safety of [ 91298-74-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335-H412
Precautionary Statements:P260-P273-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338

Application In Synthesis of [ 91298-74-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 91298-74-7 ]

[ 91298-74-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 91298-74-7 ]
  • [ 56844-12-3 ]
  • [ 1580542-00-2 ]
YieldReaction ConditionsOperation in experiment
77% In butan-1-ol; at 145℃; for 22h; General procedure: Compound 1 (1.00 g, 4.01 mmol) was mixed with the benzylamine (12.03 mmol) and 1-butanol (3.5 mL) and agitated at 145 C for 18-24 h. Then the mixture was cooled to rt, diluted with water (50 mL) and diethyl ether (150 mL) or EtOAc (150 mL). After phase separation, the water phase was extracted with more diethyl ether (2 × 50 mL) or EtOAc (2 × 50 mL). The combined organic phases were washed with saturated aq NaCl solution (50 mL), dried over anhydrous Na2SO4, filtered and concentrated in vacuo, before the crude oil was dried under reduced pressure to constant weight to remove excess benzylamine. The compounds were purified by silica-gel column chromatography or crystallized as specified for each individual compound
  • 2
  • [ 876343-10-1 ]
  • [ 91298-74-7 ]
  • C15H15IN4O [ No CAS ]
 

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