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Chemical Structure| 915280-62-5 Chemical Structure| 915280-62-5

Structure of 915280-62-5

Chemical Structure| 915280-62-5

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Product Details of [ 915280-62-5 ]

CAS No. :915280-62-5
Formula : C19H23NO3
M.W : 313.39
SMILES Code : O=C1OCC(CC2=CC=CC=C2)N1C(C(CC3CCCC3)=C)=O

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Application In Synthesis of [ 915280-62-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 915280-62-5 ]

[ 915280-62-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 915280-62-5 ]
  • [ 51307-59-6 ]
  • C27H34N2O5 [ No CAS ]
YieldReaction ConditionsOperation in experiment
General procedure: O-(4-Methoxybenzyl) hydroxylamine (30 g, 0.196 mol) and 9(23 g, 0.08 mol) were mixed together under nitrogen atmosphere.The mixture was warmed to 45 C and stirred for 24 h. The resulting mixture was diluted with ethyl acetate (50 mL). p-Toluene sulphonic acid (68 g, 0.394 mol) in ethyl acetate (120 mL)was added to this solution. The resulting mixture was stirred for 1.5 h, filtered,and concentrated under reduced pressure. MTBE (550 mL) was added to this residue and stirred overnight. The resulting mixture was filtered and the filter cake added to a mixture solution of ethyl acetate (150 mL) and aqueous sodium carbonate (0.36 mol/L,150 mL). The reaction mixture was stirred for 30 min and the aqueous layer separated. The organic layer was washed with brine,dried over Na2SO4, filtered, and concentrated under reduced pressure to yield 10 (21 g, 59.6%) as a colorless oil.
 

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