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[ CAS No. 923283-54-9 ]

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Chemical Structure| 923283-54-9
Chemical Structure| 923283-54-9
Structure of 923283-54-9 * Storage: {[proInfo.prStorage]}

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Product Details of [ 923283-54-9 ]

CAS No. :923283-54-9 MDL No. :MFCD04969992
Formula : C6H9N3O2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :155.16 g/mol Pubchem ID :-
Synonyms :

Safety of [ 923283-54-9 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:1759
Hazard Statements:H314 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 923283-54-9 ]

  • Upstream synthesis route of [ 923283-54-9 ]
  • Downstream synthetic route of [ 923283-54-9 ]

[ 923283-54-9 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 923283-54-9 ]
  • [ 3473-63-0 ]
  • [ 314021-93-7 ]
YieldReaction ConditionsOperation in experiment
94% With N-ethyl-N,N-diisopropylamine In butan-1-ol at 110℃; for 1 h; Compound 8: To a solution of 7 (0.92 g, 5.9 mmol) in 5 mL of Hunig's base and 5 mL of n-butanol was added formamidine acetate (0.68 g, 6.5 mmol). The reaction mixture was heated and stirred at 110° C. for 1 hour. After cooling to room temperature, the white precipitate was collected by filtration and washed with diethyl ether. The resulting white precipitate was dried under reduced pressure to afford 8 (0.83 g, 94percent). 1H NMR (d6-DMSO) δ 4.33 (s, 3H) 8.50 (s, 1H) 8.80 (s, 1H); ES (+) MS m/e=151 (M+1).
Reference: [1] Patent: US2007/27166, 2007, A1, . Location in patent: Page/Page column 80
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