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Chemical Structure| 934-67-8 Chemical Structure| 934-67-8

Structure of 934-67-8

Chemical Structure| 934-67-8

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Product Details of [ 934-67-8 ]

CAS No. :934-67-8
Formula : C8H14O2
M.W : 142.20
SMILES Code : O=C([C@H]1CC[C@@H](C)CC1)O
MDL No. :MFCD20617670
InChI Key :QTDXSEZXAPHVBI-UHFFFAOYSA-N
Pubchem ID :20330

Safety of [ 934-67-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 934-67-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 934-67-8 ]

[ 934-67-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 934-67-8 ]
  • [ 23218-93-1 ]
  • C16H19NO6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
14.22 g (100 mmol) of compound II-1 was refluxed in 50 mL of thionyl chloride for 5 hours, The excess amount of thionyl chloride was then divisible and the resulting residue was dissolved in 20 mL of dry dichloromethane. 19.61 g (100 mmol) of compound III-1 and 30.36 g (300 mmol) of triethylamine were dissolved in dichloromethane, The mixture was stirred under ice-cooling, and then the acid chloride solution of II-1 prepared above was slowly added dropwise. After completion of the dropwise addition, Stirring was continued at room temperature overnight. The reaction mixture was poured into 500 mL of ice water, stirred, Extracted with 100 mL of X3 dichloromethane, the combined extracts were washed with brine, dried over anhydrous sodium sulfate, And then evaporated on a rotary evaporator. The resulting residue was purified by column chromatography to give pure IV-1. ESI-MS, m / z = 321 ([M + HD.
 

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