Home Cart Sign in  
Chemical Structure| 97606-39-8 Chemical Structure| 97606-39-8

Structure of 97606-39-8

Chemical Structure| 97606-39-8

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 97606-39-8 ]

CAS No. :97606-39-8
Formula : C16H17NO
M.W : 239.31
SMILES Code : CN(C1=CC=C(C(CC2=CC=CC=C2)=O)C=C1)C

Safety of [ 97606-39-8 ]

Application In Synthesis of [ 97606-39-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 97606-39-8 ]

[ 97606-39-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 178686-24-3 ]
  • [ 97606-39-8 ]
  • [ 57-13-6 ]
  • [ 1283117-63-4 ]
YieldReaction ConditionsOperation in experiment
16.3% With hydrogenchloride; In ethanol; water; for 48.0h;Reflux; 00199] To a solution of l-(4-(dimethylamino)phenyl)-2-phenylethanone (80 mg, 0.32 mmol), <strong>[178686-24-3]3-ethoxy-4-hydroxy-5-nitrobenzaldehyde</strong> (63 mg, 0.32 mmol), and urea (60 mg, 0.96 mmol) in 5 mL of ethanol was added 0.2 mL of concentrated HC1 solution, and the mixture was refluxed for 2 days. After the solvent was removed under reduced pressure, the residue was purified by reverse-phase preparatory HPLC (26-53% acetonitrile + 0.1% trifluoroacetic acid in water + 0.1% trifluoroacetic acid, over 15 min.) to give Compound 54 (27 mg, yield 16.3%). 1H NMR (DMSO- 6 400 MHz TMS): delta 10.29 (s, 1H), 8.51 (s, 1H), 7.47 (d, J = 8.8 Hz, 2H), 7.23 (s, 1H), 7.07-6.97 (m, 5H), 6.83 (d, J = 7.2 Hz, 2H), 6.58 (d, J = 8.4 Hz, 2H), 5.07 (d, J = 2.4 Hz, 1H), 4.05 (q, J = 6.8 Hz, 2H), 2.88 (s, 6H), 1.34 (t, J = 6.8 Hz, 3H); MS (ESI): m/z 475.0 [M+l]+.
 

Historical Records

Technical Information

Categories