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Chemical Structure| 99573-34-9 Chemical Structure| 99573-34-9

Structure of 99573-34-9

Chemical Structure| 99573-34-9

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Product Details of [ 99573-34-9 ]

CAS No. :99573-34-9
Formula : C9H7BrN2O
M.W : 239.07
SMILES Code : OC1=C2N=CC=CC2=C(N)C=C1Br

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Application In Synthesis of [ 99573-34-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 99573-34-9 ]

[ 99573-34-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 97-08-5 ]
  • [ 99573-34-9 ]
  • 5-amino-7-bromoquinolin-8-yl 4-chloro-3-nitrobenzenesulfonate [ No CAS ]
YieldReaction ConditionsOperation in experiment
93% With triethylamine; In tetrahydrofuran; at 0 - 20℃; for 6h; General procedure: To a mixture of 5-amino-7-bromoquinolin-8-ol (4) (1 mmol, 0.5 g) and TEA (2 mmol, 0.385 mL) in dry THF (10 ml) at 0 C, naphthalene-1-sulfonyl chloride (1 mmol, 0.47g) in dry THF was added drop wise and stirred for 6 h at room temperature. After completion, the reaction mixture was evaporated under vacuum to obtain the residue, which was purified by washings with n-hexane and diethyl ether to obtain pure product 5-amino-7-bromoquinolin-8-ylnaphthalene-1-sulfonate (0.79g) (5a).
 

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