104190-22-9|1-(2-Ethynylphenyl)ethanone| Ambeed

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Quality Control of [ 104190-22-9 ] Purity: 95% SDS Specification

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Product Details of [ 104190-22-9 ]

CAS No. :	104190-22-9
Formula :	C₁₀H₈O
M.W :	144.17
SMILES Code :	CC(C1=CC=CC=C1C#C)=O
MDL No. :	MFCD18207358
InChI Key :	YQXSJPABBZMARN-UHFFFAOYSA-N
Pubchem ID :	582213

Safety of [ 104190-22-9 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H302-H312-H332
Precautionary Statements:	P261-P264-P270-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P330-P362-P403+P233-P501

Application In Synthesis of [ 104190-22-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 104190-22-9 ]

[ 104190-22-9 ] Synthesis Path-Downstream 1~39

1
[ 104190-22-9 ]
[ 153093-72-2 ]

References: [1]Liebigs Annalen der Chemie,1993,p. 1009 - 1016.
[2]Journal of Organic Chemistry,2018,vol. 83,p. 7799 - 7813.
[3]Advanced Synthesis and Catalysis,2021,vol. 363,p. 4024 - 4032.

2
[ 69739-34-0 ]
[ 104190-22-9 ]
tert-Butyl-[1-(2-ethynyl-phenyl)-vinyloxy]-dimethyl-silane [ No CAS ]

References: [1]Tetrahedron Letters,2001,vol. 42,p. 5809 - 5812.

3
[ 111-34-2 ]
[ 104190-22-9 ]
(+/-)-(1RS,3SR,3aSR,5SR,9bSR)-3,5-methano-5-methyl-1-propyl-1,3,3a,9b-tetrahydrofuro[3,4-c]isochromene [ No CAS ]

References: [1]Journal of the American Chemical Society,2005,vol. 127,p. 2709 - 2716.
[2]Journal of the American Chemical Society,2001,vol. 123,p. 5814 - 5815.

4
[ 2678-54-8 ]
[ 104190-22-9 ]
(+/-)-(1RS,3SR,3aSR,5SR,9bSR)-1,5-dimethyl-3-ethoxy-3,5-methano-1,3,3a,9b-tetrahydrofuro[3,4-c]isochromene [ No CAS ]

References: [1]Journal of the American Chemical Society,2005,vol. 127,p. 2709 - 2716.
[2]Journal of the American Chemical Society,2001,vol. 123,p. 5814 - 5815.

5
[ 104190-22-9 ]
[ 704-00-7 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5814 - 5815.

6
[ 67-56-1 ]
[ 201230-82-2 ]
[ 104190-22-9 ]
(Z)-3-methoxy-1-[(methoxycarbonyl)methylene]-3-methyl-1,3-dihydroisobenzofuran [ No CAS ]
(E)-3-methoxy-1-[(methoxycarbonyl)methylene]-3-methyl-1,3-dihydroisobenzofuran [ No CAS ]

References: [1]European Journal of Organic Chemistry,2004,p. 574 - 585.

7
[ 67-56-1 ]
[ 201230-82-2 ]
[ 104190-22-9 ]
dimethyl 2-(2-dimethoxymethylphenyl)-but-2-enedioate [ No CAS ]

References: [1]European Journal of Organic Chemistry,2004,p. 574 - 585.

8
[ 201230-82-2 ]
[ 67-63-0 ]
[ 104190-22-9 ]
(Z)-3-isopropoxy-1-[(isopropoxycarbonyl)methylene]-3-methyl-1,3-dihydroisobenzofuran [ No CAS ]
(E)-3-isopropoxy-1-[(isopropoxycarbonyl)methylene]-3-methyl-1,3-dihydroisobenzofuran [ No CAS ]

References: [1]European Journal of Organic Chemistry,2004,p. 574 - 585.

9
[ 104190-22-9 ]
[ 153093-73-3 ]

References: [1]Liebigs Annalen der Chemie,1993,p. 1009 - 1016.

10
[ 104190-22-9 ]
8,9,12,13-tetradehydro-6,7-dihydro-5H-benzoundecen-5-one [ No CAS ]

References: [1]Liebigs Annalen der Chemie,1993,p. 1009 - 1016.

11
[ 104190-22-9 ]
[ 153093-74-4 ]

References: [1]Liebigs Annalen der Chemie,1993,p. 1009 - 1016.

12
[ 1156005-30-9 ]
[ 104190-22-9 ]
22,25-bis{2-(2-acetylphenyl)-1-ethynyl}-1,20-dioxa[7.7]paracyclophane [ No CAS ]
22,25-bis{2-(2-acetylphenyl)-1-ethynyl}-1,20-dioxa[7.7]paracyclophane [ No CAS ]

References: [1]Chemical Communications,2009,p. 1870 - 1872.

13
[ 917-64-6 ]
[ 104190-22-9 ]
2-(2-ethynyl-phenyl)-propan-2-ol [ No CAS ]

References: [1]Organic Letters,2009,vol. 11,p. 5350 - 5353.

14
1-(2-((trimethylsilyl)ethynyl)phenyl)ethanone [ No CAS ]
[ 104190-22-9 ]

Yield	Reaction Conditions	Operation in experiment
99%	With potassium carbonate; In methanol; at 20℃; for 3h;	To an eggplant flask was added 1-(2-((trimethylsilyl)ethynyl)phenyl)ethan-1-one (5.83g, 0.027mol), potassium carbonate (0.37g, 0.0027mol) and methanol , and stirred at room temperature for 3 hours. After the reaction was completed, it was quenched by adding saturated ammonium chloride solution, extracted with dichloromethane, washed with water, dried over sodium sulfate, and concentrated to obtain 1-(2-ethynylphenyl)ethan-1-one with a yield of 99%.

References: [1]Patent: CN114133336,2022,A .Location in patent: Paragraph 0081; 0085.
[2]Organic Letters,2014,vol. 16,p. 5588 - 5591.
[3]Journal of Organic Chemistry,2015,vol. 80,p. 11360 - 11368.
[4]Organic Letters,2009,vol. 11,p. 5350 - 5353.
[5]Chemical Communications,2013,vol. 49,p. 11320 - 11322.
[6]Journal of Organic Chemistry,2018,vol. 83,p. 7799 - 7813.
[7]Advanced Synthesis and Catalysis,2019,vol. 361,p. 3612 - 3618.
[8]Advanced Synthesis and Catalysis,2021,vol. 363,p. 4024 - 4032.
[9]Chinese Journal of Chemistry,2022,vol. 40,p. 46 - 52.

15
[ 3607-17-8 ]
[ 104190-22-9 ]
[ 1309565-92-1 ]

References: [1]Organic Letters,2011,vol. 13,p. 3190 - 3193.

16
[ 104190-22-9 ]
[ 1309565-80-7 ]

References: [1]Organic Letters,2011,vol. 13,p. 3190 - 3193.

17
[ 104190-22-9 ]
C₁₇H₂₂O₂ [ No CAS ]

References: [1]Chemistry - A European Journal,2013,vol. 19,p. 14787 - 14790.

18
[ 104190-22-9 ]
[ 149-73-5 ]
o-ethynylacetophenone [ No CAS ]

References: [1]Chemistry - A European Journal,2013,vol. 19,p. 14787 - 14790.

19
[ 589-87-7 ]
[ 104190-22-9 ]
1-(2-((4-bromophenyl)ethynyl)phenyl)ethan-1-one [ No CAS ]