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CAS No. : | 120173-41-3 | MDL No. : | MFCD08690086 |
Formula : | C8H5BrO2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | QAQOLRCTTDVBAK-UHFFFAOYSA-N |
M.W : | 213.03 | Pubchem ID : | 14383230 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
46% | With manganese(IV) oxide In tetrahydrofuran at 60℃; for 4 h; | Manganese dioxide (IV) (35.5 g, 408 mmol) was added to a tetrahydrofuran (250 ml) solution of (5-bromo-1,3-phenylene)dimethanol (3.60 g, 16.6 mmol) and heated at 60 °C for 4 hours. Thereafter, filtration with Celite was carried out, and the solvent was removed from the filtrate under reduced pressure. 5-bromoisophthalaldehyde (1.61 g, 46percent) was obtained as a white solid. |
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