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[ CAS No. 120173-41-3 ] {[proInfo.proName]}

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Product Details of [ 120173-41-3 ]

CAS No. :120173-41-3 MDL No. :MFCD08690086
Formula : C8H5BrO2 Boiling Point : -
Linear Structure Formula :- InChI Key :QAQOLRCTTDVBAK-UHFFFAOYSA-N
M.W : 213.03 Pubchem ID :14383230
Synonyms :

Safety of [ 120173-41-3 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 120173-41-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 120173-41-3 ]
  • Downstream synthetic route of [ 120173-41-3 ]

[ 120173-41-3 ] Synthesis Path-Upstream   1~9

  • 1
  • [ 51760-22-6 ]
  • [ 120173-41-3 ]
YieldReaction ConditionsOperation in experiment
46% With manganese(IV) oxide In tetrahydrofuran at 60℃; for 4 h; Manganese dioxide (IV) (35.5 g, 408 mmol) was added to a tetrahydrofuran (250 ml) solution of (5-bromo-1,3-phenylene)dimethanol (3.60 g, 16.6 mmol) and heated at 60 °C for 4 hours. Thereafter, filtration with Celite was carried out, and the solvent was removed from the filtrate under reduced pressure. 5-bromoisophthalaldehyde (1.61 g, 46percent) was obtained as a white solid.
Reference: [1] Tetrahedron Letters, 2000, vol. 41, # 7, p. 1015 - 1018
[2] Synthesis, 1998, # 12, p. 1742 - 1749
[3] Chemische Berichte, 1989, vol. 122, p. 1365 - 1372
[4] New Journal of Chemistry, 2009, vol. 33, # 2, p. 345 - 357
[5] Patent: JP2015/224231, 2015, A, . Location in patent: Paragraph 0071
[6] Journal of Organic Chemistry, 1993, vol. 58, # 13, p. 3582 - 3585
  • 2
  • [ 626-19-7 ]
  • [ 120173-41-3 ]
Reference: [1] Organometallics, 2012, vol. 31, # 15, p. 5307 - 5320
[2] Journal of the American Chemical Society, 2014, vol. 136, # 18, p. 6664 - 6671
[3] Journal of Organic Chemistry, 2017, vol. 82, # 15, p. 7783 - 7790
  • 3
  • [ 626-39-1 ]
  • [ 68-12-2 ]
  • [ 120173-41-3 ]
Reference: [1] Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1994, vol. 253, p. 33 - 40
[2] Journal of the American Chemical Society, 1995, vol. 117, # 20, p. 5550 - 5560
[3] Chemistry--A European Journal, 1996, vol. 2, # 3, p. 259 - 264
  • 4
  • [ 51760-21-5 ]
  • [ 120173-41-3 ]
Reference: [1] Synthesis, 1998, # 12, p. 1742 - 1749
[2] Chemische Berichte, 1989, vol. 122, p. 1365 - 1372
  • 5
  • [ 556-96-7 ]
  • [ 120173-41-3 ]
Reference: [1] Journal of Organic Chemistry, 1993, vol. 58, # 13, p. 3582 - 3585
  • 6
  • [ 51760-23-7 ]
  • [ 120173-41-3 ]
Reference: [1] Journal of Organic Chemistry, 1993, vol. 58, # 13, p. 3582 - 3585
  • 7
  • [ 23351-91-9 ]
  • [ 120173-41-3 ]
Reference: [1] Tetrahedron Letters, 2000, vol. 41, # 7, p. 1015 - 1018
[2] Patent: JP2015/224231, 2015, A,
  • 8
  • [ 99-27-4 ]
  • [ 120173-41-3 ]
Reference: [1] Synthesis, 1998, # 12, p. 1742 - 1749
  • 9
  • [ 121-91-5 ]
  • [ 120173-41-3 ]
Reference: [1] Tetrahedron Letters, 2000, vol. 41, # 7, p. 1015 - 1018
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