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CAS No. : | 1204-21-3 | MDL No. : | MFCD00000198 |
Formula : | C10H11BrO3 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | RGQNFYVSEWDUEI-UHFFFAOYSA-N |
M.W : | 259.10 | Pubchem ID : | 70997 |
Synonyms : |
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Signal Word: | Danger | Class: | 8 |
Precautionary Statements: | P260-P264-P270-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P363-P405-P501 | UN#: | 3261 |
Hazard Statements: | H302-H314 | Packing Group: | Ⅱ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
74% | In tetrahydrofuran; at 30℃; for 0.75h; | N-(2,5-dimethoxyphenyl)-4-(4-methoxyphenyl)thiazol-2-amine (7c) The reaction of the l-(4-methoxyphenyl)thiourea (365mg, 2mM) and freshly synthesized 2- bromo-l-(2,5-dimethoxyphenyl)ethanone (520mg, 2mM) in anhydrous THF at 30C for 45 mins resulted in the formation of suspension, which was filtered and dried to yield the final product (74% yield). mp 104C. MS: m/z 343 (M + 1)+. |