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Chemical Structure| 1240622-76-7 Chemical Structure| 1240622-76-7

Structure of 1240622-76-7

Chemical Structure| 1240622-76-7

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Product Details of [ 1240622-76-7 ]

CAS No. :1240622-76-7
Formula : C5H5ClN2S
M.W : 160.63
SMILES Code : SC1=NC(C)=CC(Cl)=N1
MDL No. :MFCD16988303

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Application In Synthesis of [ 1240622-76-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1240622-76-7 ]

[ 1240622-76-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 41014-43-1 ]
  • [ 1240622-76-7 ]
  • [ 1601469-45-7 ]
YieldReaction ConditionsOperation in experiment
68% General procedure: To a solution of 4-chloro-6-methylpyrimidine-2-thiol (1) (1 mmol) in dry tetrahydrofuran (6 mL), triethylamine (0.2 mL) was added and stirred for 1 h. To this, <strong>[41014-43-1]2-(chloromethyl)benzoxazole</strong> (2)/2-(chloromethyl)benzothiazole (3)/2-(chloromethyl)-1H-benzimidazole (4) (1mmol) dissolved in dry tetrahydrofuran (5 mL) was added dropwise and continued stirring at room temperature for additional 20-24 h. The reaction mixture was poured onto crushed ice. The solid separated was filtered, dried and recrystallized from ethanol.
 

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