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Chemical Structure| 128293-64-1 Chemical Structure| 128293-64-1

Structure of 128293-64-1

Chemical Structure| 128293-64-1

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Product Details of [ 128293-64-1 ]

CAS No. :128293-64-1
Formula : C10H15N3O4
M.W : 241.24
SMILES Code : CN1C=C(NC(=O)OC(C)(C)C)N=C1C(O)=O
MDL No. :MFCD03093495
InChI Key :GZBSJWBQXNCOFP-UHFFFAOYSA-N
Pubchem ID :2757226

Safety of [ 128293-64-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 128293-64-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 128293-64-1 ]

[ 128293-64-1 ] Synthesis Path-Downstream   1~4

  • 2
  • [ 128293-62-9 ]
  • [ 128293-64-1 ]
  • 3
  • [ 24424-99-5 ]
  • [ 128293-62-9 ]
  • [ 128293-64-1 ]
YieldReaction ConditionsOperation in experiment
76% To Im-3 (0. 38 g) in DMF (8 mL) and Hunig's base (2ML) was added ditert-butyl dicarbonate (0.7 ml) and the mixture stirred at 60 C for 3 hr. It was then cooled to room temperature and brine (6 ML) and ethyl ether (6 ML) were added. The ether layer was extracted with 10% citric acid, brine, saturated sodium bicarbonate, and brine (10 mL each). The ether layer was then dried over sodium sulfate and evaporated under vacuum. NAOH (1M, 5mL) in methanol was then added and solution stirred at 60 C for 1 hr. The mixture was then cooled to 0 C and neutralised with 1M HC1 to pH 2 at which a white gel was formed. The gel was collected by gravity filtration and washed with water pH=6 before it was freeze dried to yield the product as a white powder. Yield (0.41 g, 76%). 1H NMR (DMSO): 6 9.45 (bs, 1H, NH), 7.21 (bs, 1H), 3. 86 (s, 3H), 3.67 (bs, 1H, OH), 1.4 (s, 9H).
  • 4
  • C17H21N4O3Pol [ No CAS ]
  • [ 128293-64-1 ]
  • [ 77716-11-1 ]
  • [ 125238-99-5 ]
  • C66H66N19O10Pol [ No CAS ]
 

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