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Chemical Structure| 1314874-80-0 Chemical Structure| 1314874-80-0

Structure of 1314874-80-0

Chemical Structure| 1314874-80-0

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Product Details of [ 1314874-80-0 ]

CAS No. :1314874-80-0
Formula : C5H4ClN5
M.W : 169.57
SMILES Code : NC1=NN2C(C(Cl)=NC=C2)=N1
MDL No. :MFCD20727730
InChI Key :AKEJQBRNKKIWIQ-UHFFFAOYSA-N
Pubchem ID :77231010

Safety of [ 1314874-80-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H312-H332
Precautionary Statements:P280

Application In Synthesis of [ 1314874-80-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1314874-80-0 ]

[ 1314874-80-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1753-75-9 ]
  • [ 1314874-80-0 ]
  • [ 1360609-47-7 ]
YieldReaction ConditionsOperation in experiment
With caesium carbonate;tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In 1,4-dioxane; at 90℃; for 14h; Benzo[1 ,2,5]thiadiazol-5-yl-(8-chloro-[1 ,2,4]triazolo[1 ,5-a]pyrazin-2-yl)-amine ("BIO")100 mg (0.6 mmol) of 8-pyridin-3-yl-[1 ,2,4]triazolo[1 ,5-a]pyrazin-2-ylamine, mg (0.9 mmol) 5-bromo-2,1 ,3-benzothiadiazole, 68 mg (0.1 mmol) 9,9- dimethyl-4,5-bis(diphenylphosphino)xanthene , 578 mg (1.8 mmol) cesium carbonate and 34 mg bis(dibenzylideneacetone)palladium are dissolved in 1 ml dioxane and stirred at 90 C for 14 h. HPLC and LC-MS analysis show formation of the product (LCMS (method C): mass found (M+H+, 303), HPLC (method D) Rt (min): 3.07.
 

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Related Functional Groups of
[ 1314874-80-0 ]

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Related Parent Nucleus of
[ 1314874-80-0 ]

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