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[ CAS No. 1593-60-8 ]

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Chemical Structure| 1593-60-8
Chemical Structure| 1593-60-8
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Product Details of [ 1593-60-8 ]

CAS No. :1593-60-8 MDL No. :MFCD11850835
Formula : C7H9NO3S Boiling Point : -
Linear Structure Formula :- InChI Key :N/A
M.W :187.22 g/mol Pubchem ID :-
Synonyms :

Safety of [ 1593-60-8 ]

Signal Word:Danger Class:4.1
Precautionary Statements:P240-P210-P241-P264-P280-P302+P352-P370+P378-P337+P313-P305+P351+P338-P362+P364-P332+P313 UN#:1325
Hazard Statements:H315-H319-H228 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1593-60-8 ]

  • Upstream synthesis route of [ 1593-60-8 ]
  • Downstream synthetic route of [ 1593-60-8 ]

[ 1593-60-8 ] Synthesis Path-Upstream   1~2

  • 1
  • [ 98-59-9 ]
  • [ 1593-60-8 ]
YieldReaction ConditionsOperation in experiment
87.5% With hydroxylamine hydrochloride; magnesium oxide In tetrahydrofuran; methanol; water at 20℃; Hydroxylamine hydrochloride (7.2 g, 86 mmol) was dissolved in methanol (30 ml) and water (20 ml), magnesium oxide (5.1 g, 129 mmol) was added, stirred for 10 minutes, then p-toluenesulfonyl chloride (8 g, 43 mmol) in tetrahydrofuran (300 ml), stirred vigorously at room temperature, and reacted to TLC to monitor the starting material for complete reaction. The extract was filtered through Celite, dried over anhydrous magnesium sulfate and concentrated under reduced pressure to give N-hydroxy-4-methylbenzenesulfonamide (7 g, white solid) in 87.5percent yield.
Reference: [1] Patent: CN105418632, 2016, A, . Location in patent: Paragraph 0175; 0176; 0177
[2] Synlett, 2009, # 13, p. 2149 - 2153
[3] Journal of Inorganic Biochemistry, 2013, vol. 118, p. 134 - 139
[4] Journal fuer Praktische Chemie (Leipzig), 1901, vol. <2>63, p. 176[5] Chem. Zentralbl., 1901, vol. 72, # I, p. 455
[6] European Journal of Medicinal Chemistry, 1996, vol. 31, # 12, p. 1001 - 1010
[7] Organometallics, 2017, vol. 36, # 7, p. 1259 - 1268
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  • [ 66021-66-7 ]
  • [ 1593-60-8 ]
Reference: [1] Bulletin of the Chemical Society of Japan, 1980, vol. 53, # 3, p. 775 - 784
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