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Chemical Structure| 17136-35-5 Chemical Structure| 17136-35-5

Structure of 17136-35-5

Chemical Structure| 17136-35-5

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Product Details of [ 17136-35-5 ]

CAS No. :17136-35-5
Formula : C10H14ClNO2
M.W : 215.68
SMILES Code : COC(CNCC1=CC=CC=C1)=O.[H]Cl
MDL No. :MFCD02684379
InChI Key :KITLJURGIVERDS-UHFFFAOYSA-N
Pubchem ID :24192994

Safety of [ 17136-35-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 17136-35-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17136-35-5 ]

[ 17136-35-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 21345-01-7 ]
  • [ 17136-35-5 ]
  • C24H21NO6 [ No CAS ]
YieldReaction ConditionsOperation in experiment
97% With potassium carbonate; In acetone; at 55 - 60℃; for 4.0h; Add 50g 4-phenoxy phthalic anhydride and 500g acetone into a 1L three-necked flask,After stirring and dissolving, 58 g of anhydrous potassium carbonate and 54 g of N-benzylglycine methyl ester hydrochloride were added.Slowly raise the temperature to reflux, control the temperature at 5560, react for 4h, after the completion of the reaction, cool to room temperature and filter.The filter cake was washed with acetone (100 g×2) and drained until no droplets dripped to obtain 119 g of wet compound 1 potassium salt.Add 1.2 kg of purified water and 119 g of wet compound 1 potassium salt to a 2L three-necked flask, and stir to dissolve.Control the temperature at 010, adjust the pH value to 23 with 2M hydrochloric acid.Heat preservation and stirring for crystallization for 2h, and wash the filter cake with purified water (100g×2),After being sucked dry, it was dried by blowing at 50-60C for 8 hours to obtain 85 g of white solid compound 1, with a yield of 97%.
 

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