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Chemical Structure| 173853-66-2 Chemical Structure| 173853-66-2

Structure of 173853-66-2

Chemical Structure| 173853-66-2

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Product Details of [ 173853-66-2 ]

CAS No. :173853-66-2
Formula : C5H8N2
M.W : 96.13
SMILES Code : NC1=CC=CN1C
MDL No. :MFCD19204367

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Application In Synthesis of [ 173853-66-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 173853-66-2 ]

[ 173853-66-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 117-21-5 ]
  • [ 173853-66-2 ]
  • 4-chloro-2-(1-methyl-1H-pyrazol-5-yl)isoindoline-1,3-dione [ No CAS ]
YieldReaction ConditionsOperation in experiment
60% With acetic acid; at 110℃; for 4h; General procedure: The starting materials 1 and 2 were commercially available (Energy Chemical, Shanghai, China).Compound 2 (3.72 mmol) was added to a stirred solution of compound 1 (3.38 mmol) in glacial aceticacid (10 mL). The reaction mixture was then stirred at 110 C for 4 h. After completion of the reaction,the solvent was evaporated, and the residue was purified on a silica gel column chromatography andeluted with ethyl acetate/petroleum ether (bp 60-90 C) (1:3, v/v) to give compounds 3.
 

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