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Chemical Structure| 2127-03-9 Chemical Structure| 2127-03-9
Chemical Structure| 2127-03-9

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Product Details of 2,2′-Dipyridyl disulfide

CAS No. :2127-03-9
Formula : C10H8N2S2
M.W : 220.31
SMILES Code : C1(SSC2=NC=CC=C2)=NC=CC=C1
MDL No. :MFCD00006287
InChI Key :HAXFWIACAGNFHA-UHFFFAOYSA-N
Pubchem ID :65093

Safety of 2,2′-Dipyridyl disulfide

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of 2,2′-Dipyridyl disulfide

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2127-03-9 ]

[ 2127-03-9 ] Synthesis Path-Downstream   1~11

  • 1
  • [ 2637-34-5 ]
  • C10H18N2O6S [ No CAS ]
  • [ 2127-03-9 ]
  • [ 15441-06-2 ]
  • [ 119023-07-3 ]
  • 3
  • [ 2127-03-9 ]
  • [ 17469-89-5 ]
  • [ 97800-80-1 ]
  • 4
  • [ 2127-03-9 ]
  • [ 28697-11-2 ]
  • [ 206534-51-2 ]
  • 5
  • [ 2127-03-9 ]
  • [ 1857-56-3 ]
  • 3-(3-chloro-4-methoxy-phenyl)-thiopropionic acid <i>S</i>-pyridin-2-yl ester [ No CAS ]
  • 6
  • [ 2127-03-9 ]
  • [ 29022-11-5 ]
  • [ 2799-07-7 ]
  • [ 104091-09-0 ]
  • [ 108-24-7 ]
  • Fmoc-L [ No CAS ]
  • Fmoc-K [ No CAS ]
  • CH3CO-NH-[GEELLKKLEELLKKGGC]-Spy, Mw = 8700 Da [ No CAS ]
  • 7
  • [ 2127-03-9 ]
  • [ 171408-84-7 ]
  • C35H22N2S2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With n-butyllithium; In tetrahydrofuran; for 0.5h;Cooling with ice; A mixed solution of Br2 / CH3COOH was added dropwise to a reaction flask equipped with 1 mol of A,Under the condition of nitrogen protection, the bromination reaction was carried out.Then, bis-pyridine-substituted disulfide compound Py-S-S-Py was added, and n-BuLi / THF was used as a catalyst,In the low temperature dry ice bath full mixing half an hour,Compound C was obtained. Finally, a mixed solution of meta-chlorobenzoic acid mCPBA / CH2Cl2 was introduced,The mixture was stirred for 1 hour, water was added, the solid was precipitated, washed with n-hexane,Ethanol was recrystallized to give SDF-DPySO2 in 46percent yield.
  • 8
  • [ 1293-65-8 ]
  • [ 2127-03-9 ]
  • 1-bromo-2-(2-pyridylthio)ferrocene [ No CAS ]
  • 9
  • [ 2127-03-9 ]
  • [ 53339-53-0 ]
  • [ 7693-46-1 ]
  • [ 1151989-04-6 ]
  • 10
  • [ 2127-03-9 ]
  • [ 1151989-04-6 ]
  • 11
  • [ 2127-03-9 ]
  • [ 23020-15-7 ]
  • S-(pyridin-2-yl) (2S)-2-phenylcyclopropane-1-carbothioate [ No CAS ]
 

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