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Chemistry
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2-Mesityl-5,5-dimethyl-1,3,2-dioxaborinane
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Aryls Benzene Compounds Aromatic Borons

[ CAS No. 214360-78-8 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 214360-78-8
Chemical Structure| 214360-78-8
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Quality Control of [ 214360-78-8 ]

COA NMR CNMR HPLC LC-MS

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SDS Specification
Alternatived Products of [ 214360-78-8 ]

Product Details of [ 214360-78-8 ]

CAS No. :214360-78-8 MDL No. :MFCD01318178
Formula : C14H21BO2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 232.13 Pubchem ID :-
Synonyms :

Safety of [ 214360-78-8 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330 UN#:N/A
Hazard Statements:H302-H315-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 214360-78-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 214360-78-8 ]

[ 214360-78-8 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 35387-93-0 ]
  • [ 20398-06-5 ]
  • [ 214360-78-8 ]
  • [ 23676-08-6 ]
  • methyl 6-methoxy-2',4',6'-trimethylbiphenyl-3-carboxylate [ No CAS ]
Reference： [1]Tetrahedron,2000,vol. 56,p. 9655 - 9662
  • 2
  • [ 35387-93-0 ]
  • [ 214360-78-8 ]
  • [ 121-98-2 ]
  • methyl 6-methoxy-2',4',6'-trimethylbiphenyl-3-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
1: 45% 2: 19% With TlOH In benzene Heating;
Reference： [1]Chaumeil; Signorella; Le Drian [Tetrahedron, 2000, vol. 56, # 49, p. 9655 - 9662]
  • 3
  • [ 35387-93-0 ]
  • [ 214360-78-8 ]
  • methyl 6-methoxy-2',4',6'-trimethylbiphenyl-3-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
97% With silver carbonate In benzene Heating;
Reference： [1]Chaumeil; Signorella; Le Drian [Tetrahedron, 2000, vol. 56, # 49, p. 9655 - 9662]
  • 4
  • [ 149817-62-9 ]
  • [ 214360-78-8 ]
  • [ 502622-88-0 ]
Reference： [1]Dalton Transactions,2004,p. 623 - 631
  • 5
  • [ 124-38-9 ]
  • [ 214360-78-8 ]
  • [ 480-63-7 ]
Reference： [1]Angewandte Chemie - International Edition,2008,vol. 47,p. 5792 - 5795
  • 6
  • [ 576-83-0 ]
  • [ 201733-56-4 ]
  • [ 214360-78-8 ]
YieldReaction ConditionsOperation in experiment
95% With tris-(dibenzylideneacetone)dipalladium(0); 2-(2,6-dimethoxyphenyl)-1-methyl-3-(diphenylphosphino)-1H-indole; cesium acetate; In 1,4-dioxane; at 20 - 110℃; for 0.5h;Schlenk technique; Inert atmosphere; In a 20 mL Schlenk tube,Tris (dibenzylideneacetone) dipalladium (0.0046 g, 0.005 mmol) and a ligand (palladium: ligand: 0.5 mol%: 4.0 mol%) were added followed by a magnetic force with a Teflon coating Stirring sticks,The system was replaced by nitrogen protection, 0.5 mL freshly distilled 1,4-dioxane was added,Stir well while stirring for 10 minutes to form a palladium complex.Then 2,4,6-triethylbenzene bromide (0.5 mmol) was added under nitrogen,Neopentyl glycol boronate (0.6 mmol) and cesium acetate (1.5 mmol) were added.Finally 1,4-dioxane solution (1 ml) was added and stirring was continued for 5 minutes at room temperature.The Schlenk tube was then placed in a preheated 110 C oil bath for 30 minutes. After the reaction is completed,After cooling the reaction tube to room temperature and detecting the consumption of the aryl chloride by thin layer chromatography, the reaction was stopped,About 10 ml of water was added to the system, about 10 ml of ethyl acetate was added, and the organic layer was subjected to gas chromatography.Thereafter, about 10 ml of ethyl acetate was further added in three to four times, and the organic phase was combined and concentrated under reduced pressure.Column chromatography products Neopentyl glycol 2,4,6-trimethylbenzeneboronate, isolated yield 95%
Reference： [1]Patent: CN104327106,2017,B .Location in patent: Paragraph 0029; 0030
[2]Angewandte Chemie - International Edition,2009,vol. 48,p. 5350 - 5354
    Angew. Chem., Int. Ed.,2009,vol. 121,p. 5454 - 5458
  • 7
  • [ 52742-32-2 ]
  • [ 75732-01-3 ]
  • [ 214360-78-8 ]
  • [ 137129-03-4 ]
Reference： [1]Angewandte Chemie - International Edition,2012,vol. 51,p. 3642 - 3645

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