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Chemical Structure| 23133-37-1 Chemical Structure| 23133-37-1

Structure of 23133-37-1

Chemical Structure| 23133-37-1

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Product Details of [ 23133-37-1 ]

CAS No. :23133-37-1
Formula : C8H15NO
M.W : 141.21
SMILES Code : O=C1CCN(CCC)CC1
MDL No. :MFCD00010433
InChI Key :YGDZKYYCJUNORF-UHFFFAOYSA-N
Pubchem ID :90006

Safety of [ 23133-37-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 23133-37-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 23133-37-1 ]

[ 23133-37-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 23133-37-1 ]
  • CH3 [ No CAS ]
  • [ 1336-21-6 ]
  • [ 32566-01-1 ]
  • 1'-Propyl-5,6-dihydrospiro[1H-indolo[3,2-c]quinoline-6,4'-piperidine]maleate [ No CAS ]
YieldReaction ConditionsOperation in experiment
With acetic acid; In ethanol; EXAMPLE 9 1'-Propyl-5,6-dihydrospiro[1H-indolo[3,2-c]quinoline-6,4'-piperidine]maleate, monoethanolate To a mixture prepared from 7.8 g of <strong>[32566-01-1]2-(2-aminophenyl)indole</strong>, 100 ml of ethanol and 2.5 ml of acetic acid was added 5.7 ml of 1-propyl-4-piperidone. The mixture was heated at reflux for 6 hours. The solution was cooled, concentrated and treated with a dilute NH4 OH solution. The resultant solid was collected, washed with water and dried to give 11.8 g of tan solid. This was flash chromatographed using 5% CH3 OH/CH2 Cl2 as an eluent to give 2.8 g of light tan solid. The maleate salt was prepared in ethanol and recrystallized from ethanol to give 2.2 g of solid, m.p. 150-153 dec. Analysis. Calculated for C22 H25 N3 *C4 H4 O4 *C2 H6 O: 68.13% C, 7.15% H, 8.51% N. Found: 68.00% C, 7.06% H, 8.49% N.
 

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