258332-57-9|Ethyl 2-((3-((tert-butoxycarbonyl)amino)propyl)amino)acetate| Ambeed

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Quality Control of [ 258332-57-9 ] Purity: 95% SDS Specification

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Product Details of [ 258332-57-9 ]

CAS No. :	258332-57-9
Formula :	C₁₂H₂₄N₂O₄
M.W :	260.33
SMILES Code :	O=C(OCC)CNCCCNC(OC(C)(C)C)=O
MDL No. :	MFCD06797071
InChI Key :	IUZPINCLTDROJL-UHFFFAOYSA-N
Pubchem ID :	44630168

Safety of [ 258332-57-9 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H302-H315-H319-H335
Precautionary Statements:	P261-P305+P351+P338

Application In Synthesis of [ 258332-57-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 258332-57-9 ]

[ 258332-57-9 ] Synthesis Path-Downstream 1~35

1
[ 602-94-8 ]
[ 258332-57-9 ]
[ 367955-16-6 ]

References: [1]Journal of the Chemical Society. Perkin Transactions 1 (2001),2001,p. 1605 - 1611.

2
[ 75178-96-0 ]
[ 105-39-5 ]
[ 258332-57-9 ]

References: [1]Journal of the Chemical Society. Perkin Transactions 1 (2001),2001,p. 1605 - 1611.

3
[ 367954-99-2 ]
[ 258332-57-9 ]
[ 367955-18-8 ]

References: [1]Journal of the Chemical Society. Perkin Transactions 1 (2001),2001,p. 1605 - 1611.

4
[ 258332-57-9 ]
[ 1583-58-0 ]
{N-[3-(tert-Butoxycarbonylamino)propyl]-N-(2,4-difluorobenzoyl)amino}acetic acid ethyl ester [ No CAS ]

References: [1]Journal of the Chemical Society. Perkin Transactions 1 (2001),2001,p. 1605 - 1611.

5
[ 24424-99-5 ]
[ 258332-57-9 ]
[ 352284-59-4 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

6
[ 75178-96-0 ]
[ 105-36-2 ]
[ 258332-57-9 ]

Yield	Reaction Conditions	Operation in experiment
		General procedure: Tert-butyl (5-aminoethyl)carbamate (11.7 g) was dissolved in THF (110 mL), and then Et3N (16 mL, 3.0 equiv) was added to the solution under stirring. The mixture was kept at room temperature (rt) for 10 min. Ethyl bromoacetate (12.24 mL, 1 equiv) was dissolved in THF (100 mL) and added dropwise to the solution under stirring. The mixture was kept at rt for 16 h. The mixture was concentrated in vacuo, and then the residue redissolved in Et2O (300 mL) and filtered. The filtrate was concentrated in vacuo to afford the intermediate ethyl ester (17.65 g) as a colourless oil, which was dissolved in dioxane (100 mL) and MeOH (40 mL). Then, 4M NaOH (18 mL) was added dropwise under stirring. The mixture was kept at rt for 1 h, then concentrated in vacuo, and the residue redissolved in H2O (100 mL). Fmoc-OSu (23.69 g, 1 equiv) was dissolved in warm (45 C) MeCN (170 mL) and added dropwise to the mixture under stirring. The mixture was kept at rt for 16 h, then concentrated in vacuo until it turned turbid. Then EtOAc (300 mL) was added, and the resulting mixture was washed with 10% citric acid (400 mL). The aqueous phase was extracted with EtOAc (2 × 150 mL), and the combined organic phases were washed with H2O (3 × 250 mL), and brine (250 mL). The organic phase was extracted with 10% NaHCO3-10% Na2CO3-dioxane 3:3:2 (4 × 400 mL). The combined aqueous phases were adjusted to pH 2-3 with 4M HCl, extracted with EtOAc (150 mL), then combined, dried over Na2SO4and concentrated in vacuo. The resulting solid was recrystallised from EtOAc (200 mL) and heptane (800 mL) to afford building block17(25.0 g, 77.6%) as a white solid; tR= 6.53 min. (gradient 30-100% B during 10 min).

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.
[2]Journal of Organic Chemistry,2015,vol. 80,p. 9185 - 9191.
[3]Molecules,2019,vol. 24.

7
[ 24424-99-5 ]
[ 258332-57-9 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.
[2]Journal of Organic Chemistry,2015,vol. 80,p. 9185 - 9191.

8
[ 258332-57-9 ]
[tert-butoxycarbonyl-(3-tert-butoxycarbonylamino-propyl)-amino]-acetic acid 1-phenyl-ethyl ester [ No CAS ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

9
[ 258332-57-9 ]
[ 192124-66-6 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

10
[ 258332-57-9 ]
[ 352285-61-1 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

11
[ 258332-57-9 ]
[ 352285-59-7 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

12
[ 258332-57-9 ]
[ 352285-52-0 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

13
[ 258332-57-9 ]
[ 352285-50-8 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

14
[ 258332-57-9 ]
[ 352285-63-3 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

15
[ 258332-57-9 ]
[ 352285-54-2 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

16
[ 258332-57-9 ]
[ 352285-12-2 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

17
[ 258332-57-9 ]
[ 352285-28-0 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

18
[ 258332-57-9 ]
[ 352285-30-4 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

19
[ 258332-57-9 ]
[ 352285-32-6 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

20
[ 258332-57-9 ]
[ 352285-60-0 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

21
[ 258332-57-9 ]
[ 352285-42-8 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

22
[ 258332-57-9 ]
2-[tert-butoxycarbonyl-(3-tert-butoxycarbonylamino-propyl)-amino]-acetoxy}-propionic acid methyl ester [ No CAS ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

23
[ 258332-57-9 ]
[ 352285-58-6 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

24
[ 258332-57-9 ]
[ 352285-51-9 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

25
[ 258332-57-9 ]
[ 352285-49-5 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

26
[ 258332-57-9 ]
[ 352285-62-2 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

27
[ 258332-57-9 ]
[ 352285-53-1 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

28
[ 258332-57-9 ]
[ 352285-27-9 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

29
[ 258332-57-9 ]
[ 352285-11-1 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

30
[ 258332-57-9 ]
[ 352285-40-6 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

31
[ 258332-57-9 ]
[ 352285-29-1 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

32
[ 258332-57-9 ]
[ 352285-31-5 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

33
[ 258332-57-9 ]
[ 352285-41-7 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

34
[ 258332-57-9 ]
[ 352285-39-3 ]

References: [1]Journal of the American Chemical Society,2001,vol. 123,p. 5962 - 5973.

35
[ 258332-57-9 ]
{N-[3-(tert-Butoxycarbonylamino)propyl]-N-(2,4-difluorobenzoyl)amino}acetic acid [ No CAS ]

References: [1]Journal of the Chemical Society. Perkin Transactions 1 (2001),2001,p. 1605 - 1611.

Historical Records

Technical Information

• Acyl Group Substitution • Bouveault-Blanc Reduction • Buchwald-Hartwig C-N Bond and C-O Bond Formation Reactions • Catalytic Hydrogenation • Chan-Lam Coupling Reaction • Complex Metal Hydride Reductions • Ester Cleavage • Heat of Combustion • Hydride Reductions • Lawesson's Reagent • Leuckart-Wallach Reaction • Mannich Reaction • Petasis Reaction • Preparation of Amines • Reactions of Amines • Reactions with Organometallic Reagents • Specialized Acylation Reagents-Carbodiimides and Related Reagents • Specialized Acylation Reagents-Ketenes • Specialized Acylation Reagents-Vilsmeier Reagent • Ugi Reaction

Related Functional Groups of
[ 258332-57-9 ]

Aliphatic Chain Hydrocarbons

A756665 [191274-40-5]

2-Hydroxyethyl 2-((tert-butoxycarbonyl)amino)acetate

Similarity: 0.90

A355316 [700878-01-9]

tert-Butyl 2-((methoxycarbonyl)amino)acetate

Similarity: 0.89

A904244 [222641-11-4]

Ethyl 2-((tert-butoxycarbonyl)(ethyl)amino)acetate

Similarity: 0.86

A608070 [365546-51-6]

2-((tert-Butoxycarbonyl)amino)ethyl acetate

Similarity: 0.85

Amides

A756665 [191274-40-5]

2-Hydroxyethyl 2-((tert-butoxycarbonyl)amino)acetate

Similarity: 0.90

A355316 [700878-01-9]

tert-Butyl 2-((methoxycarbonyl)amino)acetate

Similarity: 0.89

A904244 [222641-11-4]

Ethyl 2-((tert-butoxycarbonyl)(ethyl)amino)acetate

Similarity: 0.86

A917280 [203662-91-3]

Ethyl 2-(4-((tert-Butoxycarbonyl)amino)piperidin-1-yl)acetate

Similarity: 0.85

A172536 [1393442-42-6]

tert-Butyl 2-(2-oxo-1,3-oxazinan-3-yl)acetate

Similarity: 0.85

Esters

A756665 [191274-40-5]

2-Hydroxyethyl 2-((tert-butoxycarbonyl)amino)acetate

Similarity: 0.90

A355316 [700878-01-9]

tert-Butyl 2-((methoxycarbonyl)amino)acetate

Similarity: 0.89

A904244 [222641-11-4]

Ethyl 2-((tert-butoxycarbonyl)(ethyl)amino)acetate

Similarity: 0.86

A917280 [203662-91-3]

Ethyl 2-(4-((tert-Butoxycarbonyl)amino)piperidin-1-yl)acetate

Similarity: 0.85

A172536 [1393442-42-6]

tert-Butyl 2-(2-oxo-1,3-oxazinan-3-yl)acetate

Similarity: 0.85

Amines

A756665 [191274-40-5]

2-Hydroxyethyl 2-((tert-butoxycarbonyl)amino)acetate

Similarity: 0.90

A355316 [700878-01-9]

tert-Butyl 2-((methoxycarbonyl)amino)acetate

Similarity: 0.89

A904244 [222641-11-4]

Ethyl 2-((tert-butoxycarbonyl)(ethyl)amino)acetate

Similarity: 0.86

A917280 [203662-91-3]

Ethyl 2-(4-((tert-Butoxycarbonyl)amino)piperidin-1-yl)acetate

Similarity: 0.85

A608070 [365546-51-6]

2-((tert-Butoxycarbonyl)amino)ethyl acetate

Similarity: 0.85

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H420	Harms public health and the environment by destroying ozone in the upper atmosphere

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CAS No.: 258332-57-9

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