Home Cart Sign in  
Chemical Structure| 26872-48-0 Chemical Structure| 26872-48-0

Structure of 26872-48-0

Chemical Structure| 26872-48-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 26872-48-0 ]

CAS No. :26872-48-0
Formula : C18H15NO2
M.W : 277.32
SMILES Code : O=C(C1=C2C=CC=NC2=C(OCC3=CC=CC=C3)C=C1)C

Safety of [ 26872-48-0 ]

Application In Synthesis of [ 26872-48-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 26872-48-0 ]

[ 26872-48-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 2598-31-4 ]
  • [ 100-39-0 ]
  • [ 26872-48-0 ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate; In acetone; for 14h;Heating / reflux; Example 2Preparation of 5-acetyl-8-benzyloxyquinoline (compound (Ic); Ri = benzyl) <n="39"/>A 5 liter 4-necked flask equipped with a mechanical stirrer, thermometer, addition funnel and refluxing condenser was charged with <strong>[2598-31-4]5-acetyl-8-hydroxyquinoline</strong> (300 gms/1.44 moles) and acetone (3 liters). To this solution was added anhydrous potassium carbonate (443 gms/1.6 moles) in 30 minutes followed by benzyl bromide (229 ml/1.92 moles) slowly in 90 minutes. The resulting slurry was heated to reflux for 12 hours. The reaction mass was filtered through hyflo bed, after completion of reaction and washed with hot ethyl acetate (300 ml). The clear filtrate was distilled out completely at 55-600C under high vacuum. The residue was dissolved in acetone (300ml) and warmed to 500C for 5-10 minutes, cooled to 25-30C, chilled further to 0-50C and stirred for 30 minutes. The resulting 5-Acetyl-8-benzyloxyquinoline was isolated by filtration and washed with 1 :1 mixture of acetone and diisopropyl ether (150 ml) and dried under vacuum at 60-65Cfor 4-5 hours. Yield- 202 gms
  • 2
  • [ 26872-48-0 ]
  • [ 530084-79-8 ]
 

Historical Records

Technical Information

Categories