[ CAS No. 2923-28-6 ]

Name: 2923-28-6|Silver(I) trifluoromethanesulfonate|98%
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Quality Control of [ 2923-28-6 ]

COA NMR CNMR HPLC LC-MS

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Product Details of [ 2923-28-6 ]

CAS No. :	2923-28-6	MDL No. :	MFCD00013226
Formula :	CAgF₃O₃S	Boiling Point :	162°C at 760 mmHg
Linear Structure Formula :	-	InChI Key :	N/A
M.W :	256.94 g/mol	Pubchem ID :	76223
Synonyms :

Safety of [ 2923-28-6 ]

Signal Word:	Danger	Class:	8
Precautionary Statements:	P264-P280-P302+P352-P305+P351+P338+P310-P332+P313-P362+P364	UN#:	1759
Hazard Statements:	H315-H318	Packing Group:	Ⅲ
GHS Pictogram:

Application In Synthesis of [ 2923-28-6 ]

Upstream synthesis route of [ 2923-28-6 ]
Downstream synthetic route of [ 2923-28-6 ]

[ 2923-28-6 ] Synthesis Path-Upstream 1~13

1
[ 2923-28-6 ]
[ 74-88-4 ]
[ 333-27-7 ]

Reference： [1] Journal of Organic Chemistry, 1974, vol. 39, # 26, p. 3875 - 3877
[2] Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry, [3] Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980, p. 2887 - 2891
[4] , Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.1, page 48 - 120,
[5] Journal of Organic Chemistry, 1974, vol. 39, # 26, p. 3875 - 3877
[6] Journal of the Chemical Society, [7] Journal of the Chemical Society, 1956, p. 173 - 180
[8] , Gmelin Handbook: F: PerFHalOrg.2, 1.3.1, page 76 - 99,
[9] Patent: US2018/298037, 2018, A1, . Location in patent: Paragraph 0080-0083

2
[ 2923-28-6 ]
[ 18162-48-6 ]
[ 69739-34-0 ]

Reference： [1] Journal of the American Chemical Society, 1982, vol. 104, # 22, p. 6092 - 6099

3
[ 123-91-1 ]
[ 7440-55-3 ]
[ 17455-13-9 ]
[ 2923-28-6 ]
[ 1195-66-0 ]

Reference： [1] Journal of the American Chemical Society, 2016, vol. 138, # 40, p. 13119 - 13122

4
[ 123-91-1 ]
[ 7440-55-3 ]
[ 17455-13-9 ]
[ 1125-88-8 ]
[ 2923-28-6 ]
[ 72824-04-5 ]
[ 22039-97-0 ]
[ 1195-66-0 ]

Reference： [1] Journal of the American Chemical Society, 2016, vol. 138, # 40, p. 13119 - 13122

5
[ 1483-72-3 ]
[ 2923-28-6 ]
[ 66003-76-7 ]

Reference： [1] Tetrahedron, 2000, vol. 56, # 6, p. 855 - 863

6
[ 1493-13-6 ]
[ 20667-12-3 ]
[ 2923-28-6 ]

Reference： [1] Dalton Transactions, 2014, vol. 43, # 4, p. 1589 - 1598
[2] Polyhedron, 1996, vol. 15, # 24, p. 4349 - 4354
[3] Journal of the Chemical Society, [4] Journal of the Chemical Society, 1955, p. 2901 - 2910
[5] Journal of the Chemical Society, [6] Journal of the Chemical Society, 1956, p. 173 - 180
[7] Journal of the Chemical Society, [8] Journal of the Chemical Society, 1957, p. 2640 - 2645
[9] C.A., 1956, p. 13982
[10] Patent: US2732398, 1954, ,
[11] Journal of the Chemical Society, [12] Journal of the Chemical Society, 1954, p. 4228 - 4232
[13] , Gmelin Handbook: F: PerFHalOrg.2, 1.3.1, page 76 - 99,
[14] Chemistry - A European Journal, 2015, vol. 21, # 28, p. 10070 - 10081

7
[ 1493-13-6 ]
[ 2923-28-6 ]

Reference： [1] Patent: US3962224, 1976, A,

8
[ 1493-13-6 ]
[ 2923-28-6 ]

Reference： [1] Zeitschrift fuer Physikalische Chemie (Muenchen, Germany), 1983, vol. 138, p. 137 - 156
[2] C.A., 1976, vol. 85, p. 28372
[3] Thermochimica Acta, [4] Thermochimica Acta, 1993, vol. 223, p. 207 - 212
[5] , Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.1, page 48 - 120,

9
[ 563-63-3 ]
[ 2923-28-6 ]

Reference： [1] Journal of Organometallic Chemistry, 2000, vol. 600, # 1-2, p. 112 - 117

10
[ 2923-28-6 ]
[ 106-93-4 ]
[ 18928-34-2 ]
[ 103935-47-3 ]

Reference： [1] Journal of Fluorine Chemistry, 1985, vol. 29, p. 123

11
[ 2923-28-6 ]
[ 34946-82-2 ]

Reference： [1] Journal of Physical Chemistry B, 2005, vol. 109, # 48, p. 22890 - 22898

12
[ 2923-28-6 ]
[ 2926-29-6 ]
[ 811-68-7 ]

Yield	Reaction Conditions	Operation in experiment
84%	With tri-tert-butyl phosphine In acetonitrile at 0 - 20℃; for 12 h; Inert atmosphere	Under a nitrogen atmosphere, AgOTf (25.69 g, 100 mmol) and CF3SO2Na (18.73 g, 120 mmol) was dissolved in anhydrous acetonitrile (400 mL), the reaction solution was cooled to 0°C followed by the addition of tBu3P (50.58 g,250 mmol). The reaction solution was returned to room temperature, and stirred well at room temperature for 12 hours. After the reaction, the reaction solution was filtered through celite, the filtrate was cooled to -20 ° C, and crystals were precipitated. The supernatant was purged to remove most of the tri-tert-butylphosphine oxide. The supernatant was removed in vacuo to remove the solvent. The residue was washed thoroughly with ether, vacuum-dried and the residual solid was recrystallized from tetrahydrofuran and toluene to give the product trifluoromethylthio silver(I) (17.55 g, yield 84percent).

Reference： [1] Patent: CN105017110, 2016, B, . Location in patent: Paragraph 0037; 0038

13
[ 2923-28-6 ]
[ 58479-61-1 ]
[ 92886-86-7 ]

Reference： [1] Tetrahedron, 2004, vol. 60, # 38, p. 8375 - 8396
[2] Organic Letters, 2006, vol. 8, # 24, p. 5649 - 5652

[ 2923-28-6 ] Synthesis Path-Downstream 1~15

1
[ 15617-18-2 ]
[ 7732-18-5 ]
[ 2923-28-6 ]
[ 148461-16-9 ]
Pd(H₂O)2((C₆H₅)2PC₆H₄(C₃H₃(C(CH₃)3)NO))⁽²⁺⁾*2CF₃SO₃^(1-)=[Pd(H₂O)2((C₆H₅)2PC₆H₄(C₃H₃(C(CH₃)3)NO))](CF₃SO₃)2 [ No CAS ]

Reference： [1]Inorganica Chimica Acta,1999,vol. 296,p. 45 - 51

2
chloro(1,5-cyclooctadiene)rhodium(I) dimer [ No CAS ]
[ 22795-99-9 ]
[ 2923-28-6 ]
[Rh(cycloocta-1,5-diene)((-)-(S)-2-(aminomethyl)-1-ethylpyrrolidine)]CF₃SO₃ [ No CAS ]

Reference： [1]Helvetica Chimica Acta,2003,vol. 86,p. 1753 - 1759

3
[ 104413-90-3 ]
[ 67-66-3 ]
[ 2923-28-6 ]
[ 4385-76-6 ]
[ 75-05-8 ]
[ 1040733-26-3 ]
[PtCl(4-pyridylbenzoic acid)(1,1'-bis(diphenylphosphino)ferrocene)](trifluoromethanesulfonate)*0.75Et₂O*0.25chloroform [ No CAS ]

Reference： [1]Inorganic Chemistry,2008,vol. 47,p. 6464 - 6474

4
[ 1050443-03-2 ]
[ 2923-28-6 ]
[ 113682-56-7 ]
[Cp(*)4Ir4(μ-chloranilato)2(μ-1,4-bis(4-pyridyl)benzene)2](triflate)4 [ No CAS ]

Reference： [1]Organometallics,2008,vol. 27,p. 4088 - 4097

5
dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer [ No CAS ]
[ 2645-22-9 ]
[ 2923-28-6 ]
[Cp(*)Rh(μ-4,4'-dipyridyldisulfide)Cl]2(OTf)2 [ No CAS ]

Reference： [1]Dalton Transactions,2010,vol. 39,p. 7119 - 7124

6
[ 2645-22-9 ]
[ 52462-29-0 ]
[ 2923-28-6 ]
[(p-cymene)Ru(μ-4,4'-dipyridyldisulfide)Cl]2(OTf)2 [ No CAS ]

Reference： [1]Dalton Transactions,2010,vol. 39,p. 7119 - 7124

7
[ 12354-84-6 ]
[ 2645-22-9 ]
[ 2923-28-6 ]
[Cp(*)Ir(μ-4,4'-dipyridyldisulfide)Cl]2(OTf)2 [ No CAS ]

Reference： [1]Dalton Transactions,2010,vol. 39,p. 7119 - 7124

8
[ 2645-22-9 ]
3,3'-bis(2,4,6-tri-methylphenyl)-[(1,1'-diimidazolin-2,2'-diylidene)-methane]-palladium(II) dibromide [ No CAS ]
[ 2923-28-6 ]
[(1,1'-dimesityl-3,3'-methylenediimidazolin-2,2'-diylidene)Pd(4,4'-dithiodipyridine)]2(OTf)4 [ No CAS ]

Reference： [1]Organometallics,2010,vol. 29,p. 4842 - 4848

9
[ 2645-22-9 ]
[ 14783-09-6 ]
[ 7732-18-5 ]
[ 2923-28-6 ]
[(copper(II)(1,10-phenanthroline)(trifruoromethanesulfonate)2)2(μ-4,4'-dithiodipyridine)2] [ No CAS ]
[(copper(II)(1,10-phenanthroline)(trifruoromethanesulfonate)2)2(μ-4,4'-dithiodipyridine)2]*0.13H2O [ No CAS ]

Reference： [1]Zeitschrift fur Anorganische und Allgemeine Chemie,2011,vol. 637,p. 94 - 101

10
[ 67-56-1 ]
dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer [ No CAS ]
[ 60-29-7 ]
Na₂(Cu(o-phenylenebis(oxamato))) [ No CAS ]
[ 7732-18-5 ]
[ 2923-28-6 ]
[ 113682-56-7 ]
12C₁₀H₁₅^(1-)*12Rh⁽³⁺⁾*6Cu⁽²⁺⁾*6C₁₀H₄N₂O₆^(4-)*6H₂O*17CH₄O*12CF₃O₃S^(1-)*2C₄H₁₀O*6C₁₆H₁₂N₂ [ No CAS ]

Reference： [1]Journal of the American Chemical Society,2013,vol. 135,p. 8125 - 8128

11
[Pd(η³-2-Me-C₃H₄)(μ-Cl)]₂ [ No CAS ]
[ 2923-28-6 ]
[ 13406-29-6 ]
(bis(tris(4-trifluoromethylphenyl))phosphino)palladium(η3-methallyl) triflate [ No CAS ]

Reference： [1]Journal of the American Chemical Society,2015,vol. 137,p. 7371 - 7378

12
dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer [ No CAS ]
[ 17217-57-1 ]
[ 2923-28-6 ]
C₂₂H₂₇ClN₂O₂Rh⁽¹⁺⁾*CF₃O₃S^(1-) [ No CAS ]

Reference： [1]European Journal of Inorganic Chemistry,2017,vol. 2017,p. 3024 - 3029

13
[ 14096-51-6 ]
[ 2923-28-6 ]
[ 113682-56-7 ]
[(ethylenediamine)Pt(4,4′-1,4-phenylenebipyridine)]₄[trifluoromethanesulfonate]₈ [ No CAS ]

Reference： [1]Journal of the American Chemical Society,2017,vol. 139,p. 16913 - 16922

14
dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer [ No CAS ]
1,2,3‐triazole‐4,5‐dicarboxylate [ No CAS ]
[ 2923-28-6 ]
[ 113682-56-7 ]
C₈₀H₈₈N₁₀O₈Rh₄⁽²⁺⁾*2CF₃O₃S^(1-)*CH₄O [ No CAS ]

Reference： [1]Applied Organometallic Chemistry,2019,vol. 33

15
[(η⁶-p-cymene)RuCl(1,4-bis(dipyrrin-5-yl)benzene)_0.5]₂ [ No CAS ]
[ 2923-28-6 ]
[ 113682-56-7 ]
4CF₃O₃S^(1-)*C₁₂₀H₁₁₂N₁₂Ru₄⁽⁴⁺⁾ [ No CAS ]

Reference： [1]Inorganic Chemistry,2019,vol. 58,p. 4491 - 4499

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[ CAS No. 2923-28-6 ]

Quality Control of [ 2923-28-6 ]

Related Doc. of [ 2923-28-6 ]

Product Details of [ 2923-28-6 ]

Safety of [ 2923-28-6 ]

Application In Synthesis of [ 2923-28-6 ]

[ 2923-28-6 ] Synthesis Path-Upstream 1~13

[ 2923-28-6 ] Synthesis Path-Downstream 1~15

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