[ CAS No. 32596-43-3 ] {[proInfo.proName]}

Name: 32596-43-3|5-Chloro-2-hydroxyisophthalaldehyde|95%
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Quality Control of [ 32596-43-3 ]

COA NMR CNMR HPLC LC-MS

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Product Details of [ 32596-43-3 ]

CAS No. :	32596-43-3	MDL No. :	MFCD00067051
Formula :	C₈H₅ClO₃	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	MYHXSDYZVOKOAT-UHFFFAOYSA-N
M.W :	184.58	Pubchem ID :	122912
Synonyms :

Safety of [ 32596-43-3 ]

Signal Word:	Warning	Class:	N/A
Precautionary Statements:	P261-P264-P270-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P330-P362-P403+P233-P501	UN#:	N/A
Hazard Statements:	H302-H312-H332	Packing Group:	N/A
GHS Pictogram:

Application In Synthesis of [ 32596-43-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 32596-43-3 ]

[ 32596-43-3 ] Synthesis Path-Downstream 1~88

1
[ 17026-49-2 ]
[ 32596-43-3 ]

Reference： [1]Synthetic Communications,2000,vol. 30,p. 1555 - 1561
[2]Journal fur praktische Chemie (Leipzig 1954),1939,vol. <2> 152,p. 126,135
[3]Synthesis,1991,p. 325 - 326

2
[ 32596-43-3 ]
[ 77-78-1 ]
[ 98299-14-0 ]

Reference： [1]Tetrahedron,1994,vol. 50,p. 7815 - 7826

3
[ 110-52-1 ]
[ 32596-43-3 ]
1,4-Di(4-chloro-2,6-diformylphenoxy)butane [ No CAS ]

Reference： [1]Tetrahedron Letters,1995,vol. 36,p. 3889 - 3892

4
[ 32596-43-3 ]
5-<i>tert</i>-butyl-2-trimethylsilanyloxy-1,3-bis-trimethylsilanyloxymethyl-benzene [ No CAS ]
C₂₈H₃₀Cl₂O₆ [ No CAS ]
C₃₂H₃₉ClO₆ [ No CAS ]
C₄₀H₄₆Cl₂O₈ [ No CAS ]

Reference： [1]Tetrahedron Letters,2001,vol. 42,p. 1733 - 1736

5
[ 32596-43-3 ]
p-Chlorooxacalix<3>arene [ No CAS ]
p-Chlorooxacalix<4>arene [ No CAS ]

Reference： [1]Tetrahedron Letters,2001,vol. 42,p. 1733 - 1736

6
[ 32596-43-3 ]
[ 451448-47-8 ]
C₅₆H₆₇ClN₂O₅ [ No CAS ]

Reference： [1]Organic Preparations and Procedures International,2002,vol. 34,p. 552 - 558

7
[ 32596-43-3 ]
[ 24544-04-5 ]
4-chloro-2,6-bis((2,6-diisopropylphenylimino)methyl)phenol [ No CAS ]

Reference： [1]Journal of Chemical Crystallography,2003,vol. 33,p. 159 - 163

8
[ 32596-43-3 ]
[ 24544-04-5 ]
2,6-diformyl-4-chloro-phenoxy bis(2,6-diisopropylanil) [ No CAS ]

Reference： [1]Australian Journal of Chemistry,2003,vol. 56,p. 703 - 706

9
[ 32596-43-3 ]
[ 87-62-7 ]
2,6-diformyl-4-chloro-phenoxy bis(2,6-dimethylanil) [ No CAS ]

Reference： [1]Australian Journal of Chemistry,2003,vol. 56,p. 703 - 706

10
[ 32596-43-3 ]
[ 88-05-1 ]
2,6-diformyl-4-chloro-phenoxy bis(2,4,6-trimethylanil) [ No CAS ]

Reference： [1]Australian Journal of Chemistry,2003,vol. 56,p. 703 - 706

11
[ 32596-43-3 ]
C₅₆H₇₁ClN₂O₅ [ No CAS ]

Reference： [1]Organic Preparations and Procedures International,2002,vol. 34,p. 552 - 558

12
[ 32596-43-3 ]
[ 158629-89-1 ]

Reference： [1]Tetrahedron,1994,vol. 50,p. 7815 - 7826

13
[ 32596-43-3 ]
[ 158629-93-7 ]

Reference： [1]Tetrahedron,1994,vol. 50,p. 7815 - 7826

14
[ 32596-43-3 ]
tetramethyl 11,23-dichloro-25,26-dimethoxy-5,17-diazatricyclo <19.3.1.1^9,13> hexacosa-2,7,9,11,14,19,21,23,25,26-decaene-3,7,15,19-tetracarboxylate [ No CAS ]

Reference： [1]Tetrahedron,1994,vol. 50,p. 7815 - 7826

15
[ 32596-43-3 ]
hexamethyl 7-chloro-34-methoxy-1,13-diazapentacyclo <11.10.10.1^5,9.2^17,20.2^27,30> octatriaconta-3,5,7,9(34),10,15,17,19,35(36),21,25,27,29,37(38),31-pentadecaene-3,11,15,22,25,32-hexacarboxylate [ No CAS ]

Reference： [1]Tetrahedron,1994,vol. 50,p. 7815 - 7826

16
[ 32596-43-3 ]
hexamethyl 7,19,30-trichloro-3,6,37,38-trimethoxy-1,13-diazapentacyclo <11.11.11.1^5,9.1^17,21.1^28,32> octatriaconta-3,5,7,9(38),10,15,17,19,21,(37),22,26,28,30,32,(36),33-pentadecaene-3,11,15,23,26,34-hexacarboxylate [ No CAS ]

Reference： [1]Tetrahedron,1994,vol. 50,p. 7815 - 7826

17
[ 32596-43-3 ]
[ 117750-86-4 ]

Reference： [1]Journal of Heterocyclic Chemistry,1988,vol. 25,p. 145 - 154

18
[ 32596-43-3 ]
[ 61440-32-2 ]
[ 164979-01-5 ]

Yield	Reaction Conditions	Operation in experiment
	With potassium carbonate; In N-methyl-acetamide; water;	1) A mixture of <strong>[32596-43-3]2,6-diformyl-4-chlorophenol</strong> (1.0 g, 5.4 mmol), 8-phenyloctyl chloride (1.35 g, 6 mmol) and anhydrous potassium carbonate (0.83 g, 6 mmol) in dry dimethylformamide was heated to 140 C. for 6 hours. After cooling to room temperature, water (29 ml) was added and the mixture extracted with ethyl acetate (20 ml). The extracts were washed with 2M sodium hydroxide (2*10 ml), water (10 ml), dried, filtered and evaporated to a brown oil. Chromatography on flash silica eluding with diethyl ether gave 5-chloro-2-(8-phenyloctyloxy)-3-benzenedicarboxaldehyde as a pale yellow oil (2 g).

Reference： [1]Patent: US5428065,1995,A

19
copper(II) choride dihydrate [ No CAS ]
[ 13881-91-9 ]
[ 32596-43-3 ]
Cu₂(La)Cl*CH₃OH [ No CAS ]

Reference： [1]Inorganica Chimica Acta,1988,vol. 141,p. 103 - 118

20
[ 871-76-1 ]
[ 32596-43-3 ]
uranyl acetate [ No CAS ]
[ 100852-45-7 ]

Reference： [1]Inorganica Chimica Acta,1985,vol. 110,p. 181 - 190

21
[ 871-76-1 ]
[ 32596-43-3 ]
uranyl(VI) acetate dihydrate [ No CAS ]
[ 100852-45-7 ]

Reference： [1]Inorganica Chimica Acta,1986,vol. 114,p. 111 - 118

22
copper(II) acetate dihydrate [ No CAS ]
[ 13881-91-9 ]
[ 32596-43-3 ]
Cu₂(La)OH*MeOH [ No CAS ]

Reference： [1]Inorganica Chimica Acta,1988,vol. 141,p. 103 - 118

23
copper(II) acetate dihydrate [ No CAS ]
[ 6323-97-3 ]
[ 32596-43-3 ]
Cu₂(H₂Lc)OH*H₂O*CH₃OH [ No CAS ]

Reference： [1]Inorganica Chimica Acta,1988,vol. 141,p. 103 - 118

24
manganese(II) acetate hexahydrate [ No CAS ]
[ 107-35-7 ]
[ 32596-43-3 ]
Mn₂(Lb)OH*H₂O*CH₃OH [ No CAS ]

Reference： [1]Inorganica Chimica Acta,1988,vol. 141,p. 103 - 118

25
dysprosium(III) nitrate hydrate [ No CAS ]
gadolinium nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
DyGd(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*2H₂O [ No CAS ]

Reference： [1]Journal of the Chemical Society, Dalton Transactions,
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999),1990,p. 647 - 656

26
dysprosium(III) nitrate hydrate [ No CAS ]
lanthanum(III) nitrate hydrated [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
LaDy(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*H₂O [ No CAS ]

Reference： [1]Journal of the Chemical Society, Dalton Transactions,
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999),1990,p. 647 - 656

27
dysprosium(III) nitrate hydrate [ No CAS ]
europium(III) nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
DyEu(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*H₂O [ No CAS ]

Reference： [1]Journal of the Chemical Society, Dalton Transactions,
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999),1990,p. 647 - 656

28
dysprosium(III) nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
Dy₂(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*H₂O [ No CAS ]

Reference： [1]Journal of the Chemical Society, Dalton Transactions,
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999),1990,p. 647 - 656
[2]Journal of the Chemical Society, Dalton Transactions,
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999),1990,p. 647 - 656

29
gadolinium nitrate hydrate [ No CAS ]
lanthanum(III) nitrate hydrated [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
LaGd(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*2H₂O [ No CAS ]

Reference： [1]Journal of the Chemical Society, Dalton Transactions,
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999),1990,p. 647 - 656

30
gadolinium nitrate hydrate [ No CAS ]
europium(III) nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
GdEu(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*2H₂O [ No CAS ]

Reference： [1]Journal of the Chemical Society, Dalton Transactions,
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999),1990,p. 647 - 656

31
gadolinium nitrate hydrate [ No CAS ]
terbium(III) nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
GdTb(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*H₂O [ No CAS ]

Reference： [1]Journal of the Chemical Society, Dalton Transactions,
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999),1990,p. 647 - 656

32
gadolinium nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
Gd₂(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*2H₂O [ No CAS ]

33
praseodymium(III) nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
Pr₂(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*2H₂O [ No CAS ]

34
lanthanum(III) nitrate hydrated [ No CAS ]
europium(III) nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
LaEu(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*2H₂O [ No CAS ]

Reference： [1]Journal of the Chemical Society, Dalton Transactions,
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999),1990,p. 647 - 656

35
lanthanum(III) nitrate hydrated [ No CAS ]
samarium(III) nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
LaSm(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*2H₂O [ No CAS ]

Reference： [1]Journal of the Chemical Society, Dalton Transactions,
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999),1990,p. 647 - 656

36
lanthanum(III) nitrate hydrated [ No CAS ]
terbium(III) nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
LaTb(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*2H₂O [ No CAS ]

Reference： [1]Journal of the Chemical Society, Dalton Transactions,
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999),1990,p. 647 - 656

37
lanthanum(III) nitrate hydrated [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
La₂(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*H₂O [ No CAS ]

38
europium(III) nitrate hydrate [ No CAS ]
terbium(III) nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
EuTb(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*2H₂O [ No CAS ]

Reference： [1]Journal of the Chemical Society, Dalton Transactions,
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999),1990,p. 647 - 656

39
europium(III) nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
Eu₂(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*H₂O [ No CAS ]

40
samarium(III) nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
Sm₂(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*H₂O [ No CAS ]

41
terbium(III) nitrate hydrate [ No CAS ]
[ 929-59-9 ]
[ 32596-43-3 ]
Tb₂(C₆H₂O(Cl)(CHNC₂H₄OC₂H₄OC₂H₄NCH))2(NO₃)4*2H₂O [ No CAS ]

42
dysprosium(III) nitrate hydrate [ No CAS ]
[ 871-76-1 ]
[ 32596-43-3 ]
Dy(C₆H₂ClO)2(CHNC₂H₄SC₂H₄NCH)2⁽¹⁺⁾*NO₃^(1-)*2H₂O=Dy(C₆H₂ClO)2(CHNC₂H₄SC₂H₄NCH)2NO₃*2H₂O [ No CAS ]

Reference： [1]Inorganica Chimica Acta,1987,vol. 129,p. 127 - 138

43
dysprosium(III) nitrate hydrate [ No CAS ]
[ 871-76-1 ]
[ 32596-43-3 ]
Dy[C₆H₂ClO(CHO)CHNC₂H₄SC₂H₄NCHC₆H₂ClO(CHO)]⁽¹⁺⁾*NO₃^(1-)*2H₂O=Dy[S(C₂H₄NCHC₆H₂ClOCHO)2](NO₃)*2H₂O [ No CAS ]

Reference： [1]Inorganica Chimica Acta,1987,vol. 129,p. 127 - 138

44
dysprosium(III) nitrate hydrate [ No CAS ]
[ 4097-89-6 ]
[ 32596-43-3 ]
copper(II) perchlorate [ No CAS ]
[ 75-05-8 ]
[DyCu(N(CH₂CH₂NCHC₆H₂(O)(Cl)CHNCH₂CH₂)3N)(CH₃)2NCHO]⁽²⁺⁾*2ClO₄^(1-)*CH₃CN=[CuDy(C₃₉H₄₃Cl₃N₉O₄)](ClO₄)2*CH₃CN [ No CAS ]

Reference： [1]Chemical Communications,2000,p. 1033 - 1034

45
terbium(III) nitrate hexahydrate [ No CAS ]
[ 4097-89-6 ]
[ 32596-43-3 ]
Tb⁽³⁺⁾*N((CH₂CH₂NCH)2C₆H₂(OH)(Cl))2((CH₂CH₂NCH)2C₆H₂(O)(Cl))N^(1-)*2NO₃^(1-)*10H₂O=[C₃₆H₄₀N₉O₇Cl₃Tb](NO₃)*9H₂O [ No CAS ]

Reference： [1]European Journal of Inorganic Chemistry,2001,p. 1063 - 1069

46
europium(III) nitrate hexahydrate [ No CAS ]
[ 4097-89-6 ]
[ 32596-43-3 ]
Eu⁽³⁺⁾*N((CH₂CH₂NCH)2C₆H₂(OH)(Cl))3N*3NO₃^(1-)*H₂O=[Eu(N((CH₂CH₂NCH)2C₆H₂(OH)(Cl))3N)(NO₃)(H₂O)](NO₃)2 [ No CAS ]

Reference： [1]European Journal of Inorganic Chemistry,2001,p. 1063 - 1069

47
europium(III) nitrate hexahydrate [ No CAS ]
[ 4097-89-6 ]
[ 32596-43-3 ]
Eu⁽³⁺⁾*N((CH₂CH₂NCH)2C₆H₂(OH)(Cl))2((CH₂CH₂NCH)2C₆H₂(O)(Cl))N^(1-)*2NO₃^(1-)*5H₂O=[C₃₆H₄₀N₉O₇Cl₃Eu](NO₃)*4H₂O [ No CAS ]

Reference： [1]European Journal of Inorganic Chemistry,2001,p. 1063 - 1069

48
[ 32596-43-3 ]
[ 6046-93-1 ]
Cu(OCHC₆H₂Cl(O)CHO)2*0.1CH₃CN [ No CAS ]

Reference： [1]Inorganica Chimica Acta,1997,vol. 256,p. 199 - 210

49
[ 32596-43-3 ]
[ 6046-93-1 ]
Cu(OCHC₆H₂Cl(O)CHO)2*H₂O*0.1CH₃CN [ No CAS ]

Reference： [1]Inorganica Chimica Acta,1997,vol. 256,p. 199 - 210

50
lanthanum(III) nitrate hexahydrate [ No CAS ]
[ 4182-44-9 ]
[ 32596-43-3 ]
La⁽³⁺⁾*((CH₂)2N((CH₂)11CH₃)(CH₂)2)(NCHC₆H₂Cl(OH)CHO)2*3NO₃^(1-)*0.5CHCl₃=La(C₃₂H₄₃Cl₂N₃O₄)(NO₃)3*0.5CHCl₃ [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
	In acetonitrile dropwise addn. of amine to 2 equiv. aldehyde, refluxinf with 1 equiv. La(NO3)3 for 3 h, standing for 3 h; evapn., treatment with CHCl3, collection (filtration), washing (CHCl3), drying (vac.); elem. anal.;

Reference： [1]Brianese; Casellato; Tamburini; Tomasin; Vigato [Inorganica Chimica Acta, 1998, vol. 272, # 1-2, p. 235 - 251]

51
uranyl nirate hexahydrate [ No CAS ]
[ 32596-43-3 ]
[ 107-15-3 ]
((CHOC₆H₂OClCHN)2HCH₂CH₂)UO₂(NO₃) [ No CAS ]