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[ CAS No. 34176-08-4 ] {[proInfo.proName]}

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Chemical Structure| 34176-08-4
Chemical Structure| 34176-08-4
Structure of 34176-08-4 * Storage: {[proInfo.prStorage]}
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Product Details of [ 34176-08-4 ]

CAS No. :34176-08-4 MDL No. :MFCD09065037
Formula : C6H4BrNaO2S Boiling Point : -
Linear Structure Formula :- InChI Key :FJSOUHVHPWODGS-UHFFFAOYSA-M
M.W : 243.05 Pubchem ID :23670685
Synonyms :

Safety of [ 34176-08-4 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 34176-08-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 34176-08-4 ]
  • Downstream synthetic route of [ 34176-08-4 ]

[ 34176-08-4 ] Synthesis Path-Upstream   1~2

  • 1
  • [ 34176-08-4 ]
  • [ 2050-48-8 ]
YieldReaction ConditionsOperation in experiment
91% With copper diacetate In acetonitrile at 60℃; for 3 h; General procedure: A mixture of the sodium arylsulfinate (1 mmol), Cu(OAc)2 (0.5 mmol)and CH3CN (1 mL) was stirred at 60 °C in air for 3 h. After this, themixture was cooled to room temperature and filtered through a filterpaper. The organic phases were evaporated under reduced pressure andthe residue was subjected to flash column chromatography (silica gel,ethyl acetate/petroleum ether = 1/10) to obtain the desired product.All products are known compounds and were characterised by 1HNMR, 13C NMR and HRMS.
Reference: [1] Journal of Chemical Research, 2014, vol. 38, # 5, p. 265 - 268
  • 2
  • [ 34176-08-4 ]
  • [ 121-44-8 ]
  • [ 90944-62-0 ]
Reference: [1] Organic Letters, 2016, vol. 18, # 13, p. 3194 - 3197
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