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[ CAS No. 34954-65-9 ] {[proInfo.proName]}

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Chemical Structure| 34954-65-9
Chemical Structure| 34954-65-9
Structure of 34954-65-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 34954-65-9 ]

CAS No. :34954-65-9 MDL No. :MFCD04114326
Formula : C9H7NO4 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 193.16 Pubchem ID :-
Synonyms :

Safety of [ 34954-65-9 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 34954-65-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 34954-65-9 ]
  • Downstream synthetic route of [ 34954-65-9 ]

[ 34954-65-9 ] Synthesis Path-Upstream   1~2

  • 1
  • [ 34954-65-9 ]
  • [ 3177-80-8 ]
Reference: [1] Journal of Organic Chemistry, 1998, vol. 63, # 20, p. 6797 - 6801
  • 2
  • [ 67-56-1 ]
  • [ 34954-65-9 ]
  • [ 5121-34-6 ]
YieldReaction ConditionsOperation in experiment
100% for 2 h; Reflux [000221] To 8-methoxy-lH-benzo[d][l,3]oxazine-2,4-dione (0.8 g, 4.1 mmol) in anhydrous methanol (25 mL), was added sodium hydroxide (0.24 g, 4.1 mmol) and the mixture was heated to reflux for 2 hours. The solution was cooled, diluted with ethyl acetate, washed with water, saturated sodium bicarbonate, then brine, and dried with sodium sulfate. It was filtered and concentrated to yield methyl 2-amino-3-methoxybenzoate (750 mg, 100percent).
Reference: [1] Patent: WO2011/35124, 2011, A1, . Location in patent: Page/Page column 83
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