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[ CAS No. 35582-08-2 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 35582-08-2
Chemical Structure| 35582-08-2
Structure of 35582-08-2 * Storage: {[proInfo.prStorage]}
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Product Details of [ 35582-08-2 ]

CAS No. :35582-08-2 MDL No. :MFCD14657178
Formula : C9H8N2O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 160.17 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 35582-08-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 35582-08-2 ]

[ 35582-08-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 63558-65-6 ]
  • [ 35582-08-2 ]
  • (5-iodo-pyrimidin-4-yl)-(3-oxazol-2-yl-phenyl)-amine [ No CAS ]
  • 2
  • [ 26452-80-2 ]
  • [ 35582-08-2 ]
  • 4-chloro-N-(3-oxazol-2-ylphenyl)pyridin-2-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
62% With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane at 100℃; for 0.5h; Microwave irradiation; Inert atmosphere; Sealed tube; regioselective reaction; 4-chloro-N-phenyl-pyridin-2-amine (3a) General procedure: Aniline (62μl, 0.68 mmol), 2,4-dichloropyridine (100 mg, 0.68 mmol), cesium carbonate (442 mg, 1.36 mmol), xantphos (47 mg, 0.08 mmol) and Pd(OAc)2 (12 mg, 0.05 mmol) were combined in a microwave tube, sealed and purged with nitrogen. Dioxane (3 mL) was then added and the reaction solution degassed with nitrogen prior to heating at 100°C for 30 minutes. The reaction mixture was then filtered and the filtrate was purified by reverse phase chromatography, utilizing a 20-65% gradient over 9 mins, with 0.5% ammonia as modifier to afford 4-chloro-N-phenyl-pyridin-2-amine
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