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Chemical Structure| 405939-28-8 Chemical Structure| 405939-28-8

Structure of 405939-28-8

Chemical Structure| 405939-28-8

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Product Details of [ 405939-28-8 ]

CAS No. :405939-28-8
Formula : C10H13IN2O2
M.W : 320.13
SMILES Code : O=C(OC(C)(C)C)NC1=NC=CC(I)=C1
MDL No. :MFCD08235129

Safety of [ 405939-28-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302
Precautionary Statements:P280-P305+P351+P338

Application In Synthesis of [ 405939-28-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 405939-28-8 ]

[ 405939-28-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 405939-28-8 ]
  • [ 552331-00-7 ]
YieldReaction ConditionsOperation in experiment
With trifluoroacetic acid; In dichloromethane; at 0 - 20℃; for 1h; To an ice-cold solution of the product from Step A above (3.84 g, 12.0 mmol) in 25 mL of dichloromethane was added trifluoroacetic acid (12 mL) dropwise. The resultant solution was allowed to warm to room temperature and, after 1 h, the volatiles were removed under reduced pressure. The residue was dissolved in water (120 ML), and the solution was neutralized by portionwise addition of sodium bicarbonate. The mixture was extracted with ethyl acetate, and the extract was washed with saturated aqueous brine, dried over magnesium sulfate and concentrated to afford an off-white solid, which was triturated with hexanes to afford the title compound as a white powder. MS 221.1 (M+1).
 

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