Home Cart Sign in  
Chemical Structure| 52372-95-9 Chemical Structure| 52372-95-9

Structure of 52372-95-9

Chemical Structure| 52372-95-9

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 52372-95-9 ]

CAS No. :52372-95-9
Formula : C10H13NO
M.W : 163.22
SMILES Code : COC1=CC=C2C(N)CCC2=C1
MDL No. :MFCD07778333

Safety of [ 52372-95-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302
Precautionary Statements:P280-P305+P351+P338

Application In Synthesis of [ 52372-95-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 52372-95-9 ]

[ 52372-95-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 98556-31-1 ]
  • [ 52372-95-9 ]
  • C18H16IN3O [ No CAS ]
YieldReaction ConditionsOperation in experiment
48% With triethylamine; In isopropyl alcohol; at 85℃; for 3h; To a solution of 5-methoxy-2,3-dihydro-1H-inden-1-amine (526 mg, 2.0 mmol) in iPrOH (20 mL) were added <strong>[98556-31-1]4-chloro-6-iodoquinazoline</strong> (580 mg, 2.0 mmol) and TEA (1.0mL). The mixture was stirred at 85 C for 3 h. All of the volatiles were evaporated and theresidue was purified by silica gel column chromatography (using petroleum ether : EtOAc= 10:1 - 2:1) to give the desired compound A29-029 as a pale yellow solid (400 mg, yield:48%). LC-MS 418 (M+H), purity 97% (UV 214 nm); ‘H NMR (DMSO-d6, 400 MHz) ö8.80 (s, 1 H), 8.55-8.52 (m, 2 H), 8.03-8.00 (dd, J, = 2.0 Hz, J2 = 8.4 Hz, 1 H), 7.47 (d, J =8.8 Hz, 1H), 7.16 (d, J = 8.4 Hz, 1 H), 6.88 (s, 1 H), 6.75-6.72 (dd, J, = 2.4 Hz, J2= 8.4 Hz,1 H), 5.93-5.90 (m, 1 H), 3.73 (s, 3 H), 3.03-3.00 (m, 1 H), 2.88-2.83 (m, 1 H), 2.56-2.51(m, 1 H), 2.07-2.03 (m, 1 H).
 

Historical Records

Technical Information

Categories