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[ CAS No. 54166-95-9 ]

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Chemical Structure| 54166-95-9
Chemical Structure| 54166-95-9
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Product Details of [ 54166-95-9 ]

CAS No. :54166-95-9 MDL No. :MFCD00234296
Formula : C7H7ClN2O Boiling Point : -
Linear Structure Formula :- InChI Key :N/A
M.W :170.60 g/mol Pubchem ID :-
Synonyms :

Safety of [ 54166-95-9 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:
Hazard Statements:H302-H312-H315-H319-H332-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 54166-95-9 ]

  • Downstream synthetic route of [ 54166-95-9 ]

[ 54166-95-9 ] Synthesis Path-Downstream   1~15

  • 1
  • [ 54166-95-9 ]
  • [ 4755-77-5 ]
  • [ 54166-68-6 ]
YieldReaction ConditionsOperation in experiment
With pyridine
37 2'-Carbamoyl-3'-chlorooxanilic acid ethyl ester. 25. EXAMPLE 37 2'-Carbamoyl-3'-chlorooxanilic acid ethyl ester. 25. 2-Amino-6-chlorobenzamide (4.26 g, 0.025 mole) is condensed with 3.1 ml (0.0275 mole) of ethyl oxalyl chloride in a manner similar to example 3, giving 5.28 g of the title compound, m.p. 190°-193° C., after crystallization from ethanol. Elemental Analysis for C11 H11 CIN2 O4: Calc'd: C, 48.8; H, 4.10; N, 10.35. Found: C, 49.08; H, 4.05; N, 10.72.
20 2'-Carbamoyl-3'-chlorooxanilic acid ethyl ester. 25 EXAMPLE 20 2'-Carbamoyl-3'-chlorooxanilic acid ethyl ester. 25 2-Amino-6-chlorobenzamide (4.26 g., 0.025 mole) is condensed with 3.1 ml. (0.0275 mole) of ethyl oxalyl chloride in a manner similar to example 12, giving 5.28 g. of the title compound, m.p. 190°-193° C., after crystallization from ethanol. Elemental Analysis for C11 H11 CLN2 O4: Calc'd: C, 48.8; H, 4.10; N, 10.35. Found: C, 49.08; H, 4.05; N, 10.72.
20 2'-Carbamoyl-3'-chlorooxanilic acid ethyl ester. 25 EXAMPLE 20 2'-Carbamoyl-3'-chlorooxanilic acid ethyl ester. 25 2-Amino-6-chlorobenzamide (4.26 g., 0.025 mole) is condensed with 3.1 ml. (0.0275 mole) of ethyl oxalyl chloride in a manner similar to example 12, giving 5.28 g. of the title compound, m.p. 190°-193° C., after crystallization from ethanol. Elemental Analysis for C11 H11 CLN2 O4: Calc'd: C, 48.8; H, 4.10; N, 10.35: Found: C, 49.08; H, 4.05; N, 10.72.
20 2'-Carbamyl-3'-chlorooxanilic acid ethyl ester. 25. EXAMPLE 20 2'-Carbamyl-3'-chlorooxanilic acid ethyl ester. 25. 2-Amino-6-chlorobenzamide (4.26 g., 0.025 mole) is condensed with 3.1 ml. (0.0275 mole) of ethyl oxalyl chloride in a manner similar to example 12, giving 5.28 g. of the title compound, m.p. 190°-193° C., after crystallization from ethanol. Elemental Analysis for C11 H11 ClN2 O4: Calc'd: C, 48.8; H, 4.10; N, 10.35. Found: C, 49.08; H, 4.05; N, 10.72.
37 2'-Carbamoyl-3'-chlorooxanilic acid ethyl ester. 25 EXAMPLE 37 2'-Carbamoyl-3'-chlorooxanilic acid ethyl ester. 25 2-Amino-6-chlorobenzamide (4.26 g, 0.025 mole) is condensed with 3.1 ml (0.0275 mole) of ethyl oxalyl chloride in a manner similar to example 3, giving 5.28 g of the title compound, m.p. 190°-193° C., after crystallization from ethanol. Elemental Analysis for C11 H11 CIN2 O4: Calc'd: C, 48.8; H, 4.10; N, 10.35. Found: C, 49.08; H, 4.05; N, 10.72.
37 2'-Carbamoyl-3'-chlorooxanilic acid ethyl ester. 25 EXAMPLE 37 2'-Carbamoyl-3'-chlorooxanilic acid ethyl ester. 25 2-Amino-6-chlorobenzamide (4.26 g, 0.025 mole) is condensed with 3.1 ml (0.0275 mole) of ethyl oxalyl chloride in a manner similar to example 3, giving 5.28 g of the title compound, m.p. 190°-193°C., after crystallization from ethanol. Elemental Analysis for C11 H11 CIN2 O4: Calc'd: C, 48.8; H, 4.10; N, 10.35. Found: C, 49.08; H, 4.05; N, 10.72.

  • 2
  • [ 54166-95-9 ]
  • [ 14301-31-6 ]
  • 2-Chloro-6-([2-(3,4-dimethoxy-phenyl)-ethylcarbamoyl]-methyl}-amino)-benzamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
32% at 160℃; for 5h;
  • 3
  • [ 54166-95-9 ]
  • [ 29671-92-9 ]
  • [ 50440-85-2 ]
YieldReaction ConditionsOperation in experiment
100% With dimethylsulfone at 160℃; for 1h;
  • 4
  • [ 63904-41-6 ]
  • [ 54166-95-9 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide In methanol Yield given;
YieldReaction ConditionsOperation in experiment
2-Chlor-6-nitro-benzonitril, Bzl., W., Fe;
  • 8
  • [ 54166-95-9 ]
  • 5-chloro-2-[3-(4-phenyl-3,6-dihydro-1(2H)-pyridinyl)propyl]-4(3H)-quinazolinone [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: pyridine / CH2Cl2 / 1.5 h / 0 °C 2: dimethylformamide / 24 h / 20 °C 3: sodium hydroxide / dioxane; H2O / 15 h / 20 °C
Multi-step reaction with 3 steps 1: pyridine / CH2Cl2 / 1.5 h / 0 °C 2: Et3N / dimethylformamide / 24 h / 20 °C 3: aq. NaOH / dioxane / 15 h / 20 °C
  • 10
  • [ 54166-95-9 ]
  • [ 78754-83-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 78 percent / 1.5 h / 190 °C 2: 97 percent / fuming HNO3, conc. H2SO4 / -10 deg C, then to room temperature, then heating, 10 min 3: 84 percent / NH3 / butan-1-ol / 24 h / 120 - 130 °C
Multi-step reaction with 3 steps 1: 78 percent / fusion 2: 97 percent / fumic HNO3, conc. H2SO4 / 1.) -10 deg C; 2.) warming 3: 84 percent / NH3 / butan-1-ol / 24 h / 140 - 150 °C / sealed vessel
  • 11
  • [ 54166-95-9 ]
  • [ 78754-82-2 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 78 percent / 1.5 h / 190 °C 2: 97 percent / fuming HNO3, conc. H2SO4 / -10 deg C, then to room temperature, then heating, 10 min
Multi-step reaction with 2 steps 1: 78 percent / fusion 2: 97 percent / fumic HNO3, conc. H2SO4 / 1.) -10 deg C; 2.) warming
  • 12
  • [ 54166-95-9 ]
  • [ 78754-85-5 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 78 percent / 1.5 h / 190 °C 2: 97 percent / fuming HNO3, conc. H2SO4 / -10 deg C, then to room temperature, then heating, 10 min 3: 67 percent / 20percent aq. tetraethylammnium hydroxide / H2O / 30 - 35 °C
Multi-step reaction with 3 steps 1: 78 percent / fusion 2: 97 percent / fumic HNO3, conc. H2SO4 / 1.) -10 deg C; 2.) warming 3: 67 percent / tetraethylammonium hydroxide / 30 - 35 °C
  • 13
  • [ 54166-95-9 ]
  • [ 78754-86-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: 78 percent / 1.5 h / 190 °C 2: 97 percent / fuming HNO3, conc. H2SO4 / -10 deg C, then to room temperature, then heating, 10 min 3: 67 percent / 20percent aq. tetraethylammnium hydroxide / H2O / 30 - 35 °C 4: 91 percent / NH3 / butan-1-ol / 2 h / 125 °C
Multi-step reaction with 4 steps 1: 78 percent / fusion 2: 97 percent / fumic HNO3, conc. H2SO4 / 1.) -10 deg C; 2.) warming 3: 67 percent / tetraethylammonium hydroxide / 30 - 35 °C 4: 91 percent / NH3 / butan-1-ol / 24 h / 130 - 140 °C / sealed vessel
  • 14
  • [ 54166-95-9 ]
  • [ 78754-87-7 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: 78 percent / 1.5 h / 190 °C 2: 97 percent / fuming HNO3, conc. H2SO4 / -10 deg C, then to room temperature, then heating, 10 min 3: 67 percent / 20percent aq. tetraethylammnium hydroxide / H2O / 30 - 35 °C 4: 89 percent / butan-1-ol / 24 h / 140 °C
Multi-step reaction with 4 steps 1: 78 percent / fusion 2: 97 percent / fumic HNO3, conc. H2SO4 / 1.) -10 deg C; 2.) warming 3: 67 percent / tetraethylammonium hydroxide / 30 - 35 °C 4: 89 percent / butan-1-ol / 24 h / 140 - 150 °C / sealed vessel
  • 15
  • [ 54166-95-9 ]
  • [ 121496-89-7 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: 78 percent / 1.5 h / 190 °C 2: 97 percent / fuming HNO3, conc. H2SO4 / -10 deg C, then to room temperature, then heating, 10 min 3: 84 percent / NH3 / butan-1-ol / 24 h / 120 - 130 °C 4: 52 percent / K2CO3 / dimethylformamide / 6 h / 60 °C
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