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Chemical Structure| 5616-32-0 Chemical Structure| 5616-32-0

Structure of 5616-32-0

Chemical Structure| 5616-32-0

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Product Details of [ 5616-32-0 ]

CAS No. :5616-32-0
Formula : C3H6N2
M.W : 70.09
SMILES Code : N#CCNC
MDL No. :MFCD00058964
InChI Key :PVVRRUUMHFWFQV-UHFFFAOYSA-N
Pubchem ID :36652

Safety of [ 5616-32-0 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H226-H315-H319-H335
Precautionary Statements:P210-P280-P301+P330+P331-P302+P352-P304+P312-P305+P351+P338
Class:3
UN#:1993
Packing Group:

Application In Synthesis of [ 5616-32-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5616-32-0 ]

[ 5616-32-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 5616-32-0 ]
  • [ 26638-43-7 ]
  • [ 99943-10-9 ]
  • 2
  • [ 24424-99-5 ]
  • [ 5616-32-0 ]
  • [ 180976-09-4 ]
YieldReaction ConditionsOperation in experiment
In ethanol; at 20℃; for 0.5h; To a solution of methylamine hydrochloride (100 mg, 1.48 mmol) in 1 mL water and 37percent formaldehyde solution (112 muL, 1.48 mmol) in a 5 ml flask was added NaCN (72.59 mg, 1.48mmol) at room temperature. After stirring 30 min at room temperature, (Boc)2O (0.32 g, 1.47mmol) in ethanol (1 mL) was added. The mixture was stirred 30 min, and extracted with dichloromethane (2 × 3 mL), washed with 3 mL brine, and dried with Na2SO4. Evaporation ofthe solvent afforded a yellow oil, which was then purified by silica gel flash chromatography(1:4 hexane/ethyl acetate) affording the product as a pale oil. 1H NMR (400 MHz, DMSO- d6)delta 4.28 (s, 2H), 2.84 (s, 2H), 1.40 (s, 9H).
 

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[ 5616-32-0 ]

Chemical Structure| 25808-30-4

A164290 [25808-30-4]

2-(Methylamino)acetonitrile hydrochloride

Reason: Free-salt