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Chemical Structure| 65079-19-8 Chemical Structure| 65079-19-8

Structure of 2-Methylquinolin-6-amine
CAS No.: 65079-19-8

Chemical Structure| 65079-19-8

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Product Details of [ 65079-19-8 ]

CAS No. :65079-19-8
Formula : C10H10N2
M.W : 158.20
SMILES Code : NC1=CC=C2N=C(C)C=CC2=C1
MDL No. :MFCD00052600
InChI Key :TYJFYUVDUUACKX-UHFFFAOYSA-N
Pubchem ID :103148

Safety of [ 65079-19-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 65079-19-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 65079-19-8 ]

[ 65079-19-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 65079-19-8 ]
  • [ 74-88-4 ]
  • [ 92-99-9 ]
YieldReaction ConditionsOperation in experiment
39% Preparation of N,N-2-trimethylquinolin-6-amine (3) A mixture of 2-methylquinolin-6-amine (2.4 g, 15.2 mmol) and NaH (2.4 g, 60.8 mmol) in DMF (60 mL) was stirred at 40 C. for 3 hrs. Then CH3I (3.8 mL, 60.8 mmol) was added by syringe. The reaction mixture was stirred at 40 C. overnight and then cooled to room temperature. The reaction mixture was diluted with water and extracted with EtOAc. The organic layer was washed with water and brine and dried over anhydrous Na2SO4. After purified by column chromatography (hexane/EtOAc=25:1), compound 3 was obtained (1.1 g, 39%). MS [M++1]=187, LC-MS: tR=0.775 min.
 

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