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Chemical Structure| 654655-69-3 Chemical Structure| 654655-69-3
Chemical Structure| 654655-69-3

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Product Details of Bedaquiline Impurity 5

CAS No. :654655-69-3
Formula : C17H14BrNO
M.W : 328.20
SMILES Code : COC1=NC2=C(C=C(Br)C=C2)C=C1CC1=CC=CC=C1
MDL No. :MFCD22493488
InChI Key :WMFHVNYOCKTDMX-UHFFFAOYSA-N
Pubchem ID :11667032

Safety of Bedaquiline Impurity 5

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of Bedaquiline Impurity 5

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 654655-69-3 ]

[ 654655-69-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 654655-69-3 ]
  • [ 21970-65-0 ]
  • C34H33BrN2O2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Compound J was prepared as follows: present intermediate 3 was reacted with intermediate compound 3 of WO 2004/011436 in the same way as described in Example B12 of WO 2004/011436. The obtained residue (4.9 g) was purified by column chromatography over silica gel (eluent: CH2Cl2). One fraction was collected and the solvent was evaporated. Yield: 1.43 g of compound J, which is a mixture of diastereoisomers.
 

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