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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 7071-83-2 Chemical Structure| 7071-83-2

Structure of 7071-83-2

Chemical Structure| 7071-83-2

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Product Details of [ 7071-83-2 ]

CAS No. :7071-83-2
Formula : C14H7ClO2
M.W : 242.66
SMILES Code : O=C(Cl)C1=CC=CC(C2=O)=C1C3=C2C=CC=C3
MDL No. :MFCD00009931

Safety of [ 7071-83-2 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314-H351
Precautionary Statements:P280-P305+P351+P338-P310
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 7071-83-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7071-83-2 ]

[ 7071-83-2 ] Synthesis Path-Downstream   1~3

  • 2
  • [ 6066-82-6 ]
  • [ 7071-83-2 ]
  • [ 6223-83-2 ]
  • N-succinimidyl-4-carboxy-9-fluorenone [ No CAS ]
  • 3
  • [ 120-95-6 ]
  • [ 6223-83-2 ]
  • [ 7071-83-2 ]
YieldReaction ConditionsOperation in experiment
With thionyl chloride; triethylamine; In hexane; toluene; Synthesis Example 1 Synthesis of Exemplary Compound (1-36) To 25 g of <strong>[6223-83-2]9-fluorenone-4-carboxylic acid</strong> is added 150 ml of thionyl chloride, followed by heating and stirring at 80 C. for 6 hours. After cooling to room temperature (25 C.), 150 ml of n-hexane is added thereto and the precipitated crystals are filtered to obtain 23 g (yield of 86%) of <strong>[6223-83-2]9-fluorenone-4-carboxylic acid</strong> chloride. Next, to a solution obtained by mixing 15.5 g of 2,4-di-t-pentylphenol, 150 ml of toluene, and 6.7 g of triethylamine is added 14.5 g of <strong>[6223-83-2]9-fluorenone-4-carboxylic acid</strong> chloride obtained above, followed by stirring at room temperature (25 C.) for 48 hours. The reactant is purified by silica gel chromatography to obtain 22 g of an exemplary compound (1-36) which is a desired product.
 

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Technical Information

• Acyl Group Substitution • Alkyl Halide Occurrence • Baeyer-Villiger Oxidation • Barbier Coupling Reaction • Baylis-Hillman Reaction • Bucherer-Bergs Reaction • Catalytic Hydrogenation • Clemmensen Reduction • Complex Metal Hydride Reductions • Corey-Bakshi-Shibata (CBS) Reduction • Corey-Chaykovsky Reaction • Fischer Indole Synthesis • General Reactivity • Grignard Reaction • Henry Nitroaldol Reaction • Hiyama Cross-Coupling Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Kinetics of Alkyl Halides • Kumada Cross-Coupling Reaction • Lawesson's Reagent • Leuckart-Wallach Reaction • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Peterson Olefination • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Aldehydes and Ketones • Preparation of Amines • Prins Reaction • Reactions of Aldehydes and Ketones • Reactions of Alkyl Halides with Reducing Metals • Reactions of Amines • Reactions of Benzene and Substituted Benzenes • Reformatsky Reaction • Robinson Annulation • Rosenmund Reduction • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Specialized Acylation Reagents-Ketenes • Stille Coupling • Stobbe Condensation • Substitution and Elimination Reactions of Alkyl Halides • Suzuki Coupling • Tebbe Olefination • Ugi Reaction • Wittig Reaction • Wolff-Kishner Reduction

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