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CAS No. : | 7149-14-6 | MDL No. : | MFCD09878135 |
Formula : | C6H3BrINO2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | CJUZKENURNQSDJ-UHFFFAOYSA-N |
M.W : | 327.90 | Pubchem ID : | 238706 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P301+P312-P302+P352-P304+P340-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
77% | With potassium iodide; sodium nitrite In water; acetonitrile at 0 - 5℃; for 0.5 h; | Ice-cold solution of sodium nitrite (57.2 g, 829 mmol) and potassium iodide (138 g, 829 mmol) in water (25 mL) was added drop wise simultaneously to a stirred suspension of 2-bromo-4-nitroaniline (60 g, 276 mmol) in acetonitrile (250 mL) at 0-5 °C and stirred for 30 minutes. The reaction mixture was then poured on to ice-cold water (1000 mL). The solid obtained was filtered, washed with water and dried to afford the titlecompound.Yield: 70.0 g (77 percent); 1H NMR (300 MHz, CDCI3): O 7.86 (dd, 1H, J= 8.7, 2.4 Hz, Ar), 8.10(d, 1H, J= 8.7 Hz, Ar), 8.45 (d, 1H, J= 2.4 Hz, Ar); MS (El, 70 eV): m/z 328.3 (M+H). |
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