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Chemical Structure| 897043-47-9 Chemical Structure| 897043-47-9

Structure of 897043-47-9

Chemical Structure| 897043-47-9

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Product Details of [ 897043-47-9 ]

CAS No. :897043-47-9
Formula : C12H21NO3
M.W : 227.30
SMILES Code : O=C(N1CC(CC=C)C(O)C1)OC(C)(C)C
MDL No. :MFCD23099256

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 897043-47-9 ]

[ 897043-47-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 897043-47-9 ]
  • [ 120871-73-0 ]
YieldReaction ConditionsOperation in experiment
50 g With Dess-Martin periodane; In dichloromethane; at 10 - 20℃; 58 g (0.26 mol) of 3-allyl-4-hydroxypyrrolidine-1-carboxylic acid tert-butyl ester was dissolved in dichloromethane,Add 120 g (0.28 mol) of Dess Martin reagent in batches at 10-20 C, and react at room temperature.TLC detects the end of the reaction.Add sodium thiosulfate solution and saturated sodium bicarbonate solution to quench the reaction and separate the liquid.The dichloromethane layer was washed with water. The crude product was subjected to flash column chromatography to obtain 50 g of the product.
 

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