There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
type | HazMat fee |
Excepted Quantity | Free |
Inaccessible (Haz class 6.1), Domestic | USD 41.00 |
Inaccessible (Haz class 6.1), International | USD 64.00 |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 83.00 |
Accessible (Haz class 3, 4, 5 or 8), International | USD 133.00 |
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CAS No. : | 938-18-1 | MDL No. : | MFCD00013650 |
Formula : | C10H11ClO | Boiling Point : | 143-146°C at 60 mmHg |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 182.65 g/mol | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Danger | Class: | 8 |
Precautionary Statements: | P280-P305+P351+P338-P310 | UN#: | 3265 |
Hazard Statements: | H314 | Packing Group: | Ⅱ |
GHS Pictogram: |
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Yield | Reaction Conditions | Operation in experiment |
---|---|---|
92.2% | Stage #1: With sodium In toluene at 65 - 70℃; for 2 h; Stage #2: at 5 - 10℃; for 1 h; Stage #3: at 70 - 75℃; for 5 h; |
In 100ml reaction flask was added toluene 32g, 3.45g of sodium metal particles (0.15mol), stirring, dropping 6.9g ethanol (0.15mol) dropwise, the process of maintaining the temperature at 65 ~ 70 ° C.Dropping end, stirring 2h, the reaction system was added dropwise phenylphosphine chloride 33. lg (0.15mol), the control temperature 5 ~ 10 ° C, the dropwise addition is complete,Stirring 1h, continue to the reaction system dropwise 2,4,6-trimethylbenzoyl chloride 30.1g (0.16mol), the dropping temperature was controlled at 70 ~ 75 ° C, and then stirred for 5h. The reaction was completed, the reaction material was added 15g of water, stirred lh, standing stratification, the resulting organic phase was adjusted to a saturated aqueous sodium bicarbonate solution pH 7 ~ 8, points to the aqueous phase, the organic phase was washed with water ,The resulting organic phase was dehydrated, cooled and crystallized, filtered,Dried to give a pale yellow powdery solid 48.2g, melting point 91 ~ 94 ° C, the liquid content of 99.3percent, a yield of 92.2percent |
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