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Chemical Structure| 948592-54-9 Chemical Structure| 948592-54-9

Structure of 948592-54-9

Chemical Structure| 948592-54-9

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Product Details of [ 948592-54-9 ]

CAS No. :948592-54-9
Formula : C12H16BClO3
M.W : 254.52
SMILES Code : OC1=CC=C(Cl)C(B2OC(C)(C)C(C)(C)O2)=C1
MDL No. :MFCD16877431
InChI Key :MTZMRMZJCYVKSJ-UHFFFAOYSA-N
Pubchem ID :53486836

Safety of [ 948592-54-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H312-H332
Precautionary Statements:P261-P264-P270-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P330-P362-P403+P233-P501

Application In Synthesis of [ 948592-54-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 948592-54-9 ]

[ 948592-54-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 948592-54-9 ]
  • [ 16427-44-4 ]
  • [ 1079402-29-1 ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate; In N,N-dimethyl acetamide; at 100℃; for 10h; Methanesulfonic acid 2-methoxyethyl ester (70.5 mg, 0.50 mmol) and 2-[2-chloro-5- hydroxyphenyl]-4,4,5,5-tetramethyl-[1 ,3,2]-dioxaborolane (Preparation 66, 100 mg, 0.42 mmol) were stirred together in N,N-dimethylacetamide (4 ml). Potassium carbonate (58 mg, 0.42 mmol) was added and the resultant solution was heated to 1000C for 10 hours. The reaction mixture was cooled then quenched with water (10 ml) and extracted with ethylacetate (10 ml).The organic layer was dried over anhydrous MgSO4 (s), filtered and evaporated in vacuo Xo give crude title compound. Material taken on without further purification.
 

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[ 948592-54-9 ]

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