392-71-2|2,6-Dichloro-4-fluorophenol| Ambeed

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Quality Control of [ 392-71-2 ] Purity: 98% SDS Specification

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Product Details of [ 392-71-2 ]

CAS No. :	392-71-2
Formula :	C₆H₃Cl₂FO
M.W :	180.99
SMILES Code :	OC1=C(Cl)C=C(F)C=C1Cl
MDL No. :	MFCD00010675
InChI Key :	BOJVIFKSTRCIRJ-UHFFFAOYSA-N
Pubchem ID :	94950

Safety of [ 392-71-2 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H315-H319
Precautionary Statements:	P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313

Application In Synthesis of [ 392-71-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 392-71-2 ]

[ 392-71-2 ] Synthesis Path-Downstream 1~41

1
[ 371-41-5 ]
[ 392-71-2 ]

References: [1]Journal of the Chemical Society,1930,p. 1870.
[2]Journal of the American Chemical Society,1959,vol. 81,p. 94,95, 97.

2
[ 392-71-2 ]
[ 697-91-6 ]

References: [1]Journal of the Chemical Society,1930,p. 1870.

3
[ 392-71-2 ]
[ 79-11-8 ]
[ 392-17-6 ]

References: [1]Journal of the American Chemical Society,1959,vol. 81,p. 94,95, 97.

4
[ 392-71-2 ]
[ 77-78-1 ]
[ 392-24-5 ]

References: [1]Journal of the Chemical Society,1930,p. 1868,2166, 2168.

5
[ 4227-95-6 ]
[ 392-71-2 ]
[ 117923-76-9 ]

References: [1]Canadian Journal of Chemistry,1988,vol. 66,p. 1635 - 1640.

6
[ 392-71-2 ]
[ 54904-42-6 ]
[ 100-02-7 ]
2,6-Cl₂-4-FC₆H₂OHgPh [ No CAS ]

References: [1]Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1975,vol. 24,p. 2334 - 2339.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1975,vol. 24,p. 2447 - 2453.

7
[ 392-71-2 ]
[ 75-03-6 ]
[ 1026397-39-6 ]

Yield	Reaction Conditions	Operation in experiment
64.9%		To a solution of 2,6-dichloro-4-fluoro-phenol (2 g, 11 .11 mmol) in 20 mL anhydrous DMF was added K2003 (3.07 g, 22.22 mmol) at room temperature. After stirring for 30 mi EtI (3.47 g, 22.22 mmol) was added and the mixture was stirred at room temperature overnight. Waterwas added and the product was extracted with MTBE. The organic phase was washed with brine, dried and concentrated in vacuum to give the crude product, which was purified by column chromatography eluted with 100 % cyclohexane to afford 1 ,3-dichloro-2-ethoxy-5-fluoro- benzene (1 .5 g, 64.9 %).1H NMR (0D013, 400MHz): ö 1.46 (t, J=7.03 Hz, 3 H) 4.07 (q, J=7.03 Hz, 2 H) 7.07 (d, J=7.78 Hz, 2 H).

References: [1]Patent: WO2015/7564,2015,A1 .Location in patent: Page/Page column 147.
[2]Journal of Medicinal Chemistry,1996,vol. 39,p. 4261 - 4274.

8
[ 392-71-2 ]
[ 79-22-1 ]
[ 183325-41-9 ]

References: [1]Chemical and Pharmaceutical Bulletin,1996,vol. 44,p. 1663 - 1668.

9
[ 371-41-5 ]
aqueous NaOCl [ No CAS ]
[ 392-71-2 ]

References: [1]Journal of the Chemical Society,1930,p. 1870.

11
[ 392-71-2 ]
[ 7697-37-2 ]
[ 697-91-6 ]

References: [1]Journal of the Chemical Society,1930,p. 1870.

12
[ 392-71-2 ]
[ 77-78-1 ]
aqueous NaOH [ No CAS ]
[ 392-24-5 ]

References: [1]Journal of the Chemical Society,1930,p. 2166,2168.

13
[ 56-23-5 ]
[ 392-71-2 ]
[ 77-78-1 ]
K₂CO₃ [ No CAS ]
[ 392-24-5 ]

References: [1]Journal of the Chemical Society,1930,p. 2166,2168.

14
[ 392-71-2 ]
[ 116133-09-6 ]
4-[4-chloro-6-(2,6-dichloro-4-fluoro-phenoxy)-[1,3,5]triazin-2-ylamino]-benzonitrile [ No CAS ]

References: [1]Bioorganic and Medicinal Chemistry Letters,2001,vol. 11,p. 2229 - 2234.

15
[ 392-71-2 ]
methyl 8-bromo-3,7-dimethyl-2,4,6-octatrienoate [ No CAS ]
[ 538315-13-8 ]

References: [1]Journal of Medicinal Chemistry,2003,vol. 46,p. 1931 - 1939.

16
[ 392-71-2 ]
[ 96-32-2 ]
[ 353556-76-0 ]

References: [1]Bioorganic and Medicinal Chemistry,2004,vol. 12,p. 2115 - 2137.

17
[ 392-71-2 ]
[ 392-17-6 ]

References: [1]Bioorganic and Medicinal Chemistry,2004,vol. 12,p. 2115 - 2137.

18
[ 392-71-2 ]
2-(2,6-dichloro-4-fluoro-phenoxy)-N-pyridin-4-yl-acetamide [ No CAS ]

References: [1]Bioorganic and Medicinal Chemistry,2004,vol. 12,p. 2115 - 2137.

19
[ 392-71-2 ]
2-(2,6-dichloro-4-fluoro-phenoxy)-N-(1H-indazol-5-yl)-acetamide [ No CAS ]

References: [1]Bioorganic and Medicinal Chemistry,2004,vol. 12,p. 2115 - 2137.

20
[ 392-71-2 ]
2-(2,6-dichloro-4-fluoro-phenoxy)-N-(1H-indazol-6-yl)-acetamide [ No CAS ]

References: [1]Bioorganic and Medicinal Chemistry,2004,vol. 12,p. 2115 - 2137.

21
[ 392-71-2 ]
(2E,4E,6E)-8-(2,6-Dichloro-4-fluoro-phenoxy)-3,7-dimethyl-octa-2,4,6-trienoic acid [ No CAS ]

References: [1]Journal of Medicinal Chemistry,2003,vol. 46,p. 1931 - 1939.

22
[ 392-71-2 ]
[ 183325-43-1 ]

References: [1]Chemical and Pharmaceutical Bulletin,1996,vol. 44,p. 1663 - 1668.

23
[ 392-71-2 ]
[ 1026303-49-0 ]